Benzoic acid, 2-[1-(4-methoxyphenyl)ethyl]hydrazide, (S)-

Base Information

Chemical Name:Benzoic acid, 2-[1-(4-methoxyphenyl)ethyl]hydrazide, (S)-
CAS No.:142068-36-8
Molecular Formula:C16H18N2O2
Molecular Weight:270.331
Hs Code.:

Synonyms:

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Chemical Property of Benzoic acid, 2-[1-(4-methoxyphenyl)ethyl]hydrazide, (S)-

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Technology Process of Benzoic acid, 2-[1-(4-methoxyphenyl)ethyl]hydrazide, (S)-

There total 10 articles about Benzoic acid, 2-[1-(4-methoxyphenyl)ethyl]hydrazide, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 613-94-5
benzoic acid hydrazide

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 142068-36-8
(R)-1-p-methoxyphenyl-1-(2-benzoylhydrazino)ethane

Guidance literature:: With nickel(II) triflate; formic acid; (S)-binapine; triethylamine; In isopropyl alcohol; at 70 ℃; enantioselective reaction; Inert atmosphere; Glovebox; Molecular sieve;
DOI:10.1002/anie.201606821

Reference yield: 96.0%

: 22454-57-5
N'-(1-(4-methoxyphenyl)ethylidene)benzohydrazide

: 142068-36-8
(R)-1-p-methoxyphenyl-1-(2-benzoylhydrazino)ethane

Guidance literature:: With formic acid; (1,2-dimethoxyethane)dichloronickel(II); triethylamine; (3S,3'S,4S,4'S,11bS,11'bS)-(+)-4,4'-di-t-butyl-4,4',5,5'-tetrahydro-3,3'-bi-3H-dinaphtho[2,1-c:1',2'-e]phosphepin; In ethanol; at 70 ℃; for 48h; stereoselective reaction;
DOI:10.1002/anie.201501018

Reference yield:

: 15151-68-5
(E)-N′-(1-(4-methoxyphenyl)ethylidene)benzohydrazide

: 142068-36-8
(S)-1-p-methoxyphenyl-1-(2-benzoylhydrazino)ethane

: 142068-36-8
(R)-1-p-methoxyphenyl-1-(2-benzoylhydrazino)ethane

Guidance literature:: With hydrogen; {(1,5-cyclooctadiene)Rh(1,2-bis((2R,5R)-2,5-diethylphospholano)benzene)}triflate; In isopropyl alcohol; at 0 ℃; for 24h; under 3102.9 Torr; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja00041a067