4'-Methoxyacetophenone benzoylhydrazone

Base Information

• Chemical Name: 4'-Methoxyacetophenone benzoylhydrazone
• CAS No.: 22454-57-5
• Molecular Formula: C16H16 N2 O2
• Molecular Weight: 268.315
• NSC Number: 166733
• DSSTox Substance ID: DTXSID60422961
• Nikkaji Number: J938.743I
• Mol file: 22454-57-5.mol

Synonyms:NSC166733;22454-57-5;DTXSID60422961;4'-Methoxyacetophenone benzoylhydrazone;NSC-166733

Chemical Property of 4'-Methoxyacetophenone benzoylhydrazone

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.09g/cm³
• XLogP3: 3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 268.121177757
• Heavy Atom Count: 20
• Complexity: 340

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=NNC(=O)C1=CC=CC=C1)C2=CC=C(C=C2)OC
• Isomeric SMILES: C/C(=N/NC(=O)C1=CC=CC=C1)/C2=CC=C(C=C2)OC

Technology Process of 4'-Methoxyacetophenone benzoylhydrazone

There total 3 articles about 4'-Methoxyacetophenone benzoylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

benzoic acid hydrazide (613-94-5) + 4-methoxyphenylacetylen (768-60-5) → N'-(1-(4-methoxyphenyl)ethylidene)benzohydrazide (22454-57-5)

Guidance literature:

With C₈₃H₆₄AuF₆N₃O₆S₂; In chlorobenzene; at 60 ℃; for 18h; Solvent; Catalytic behavior; Schlenk technique;

DOI:10.3762/BJOC.16.175

Reference yield: 83.0%

benzoic acid hydrazide (613-94-5) + 1-(4-methoxyphenyl)ethanone (100-06-1) → N'-(1-(4-methoxyphenyl)ethylidene)benzohydrazide (22454-57-5)

Guidance literature:

In ethanol; at 80 ℃; for 5h;

DOI:10.1016/j.jorganchem.2019.06.008

Reference yield:

→ N'-(1-(4-methoxyphenyl)ethylidene)benzohydrazide (22454-57-5)

Guidance literature:

p-Methoxyacetophenon IVf, Saeurehydrazid IIa;

DOI:10.1021/je60079a004

upstream raw materials:

benzoic acid hydrazide

1-(4-methoxyphenyl)ethanone

4-methoxyphenylacetylen

Downstream raw materials:

1(R)-(4-methoxyphenyl)-ethylamine

(S)-1-(4-methoxyphenyl)ethylamine

(S)-1-p-methoxyphenyl-1-(2-benzoylhydrazino)ethane

(R)-1-p-methoxyphenyl-1-(2-benzoylhydrazino)ethane

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