difluoro[4-(hydroxy-kappaO)-4-phenylbut-3-en-2-onato-kappaO]boron

Base Information

Chemical Name:difluoro[4-(hydroxy-kappaO)-4-phenylbut-3-en-2-onato-kappaO]boron
CAS No.:14871-98-8
Molecular Formula:C₁₀H₉BF₂O₂
Molecular Weight:209.988
Hs Code.:

Synonyms:STK006775;AKOS001044717;Z56871662;difluoro[4-(hydroxy-kappaO)-4-phenylbut-3-en-2-onato-kappaO]boron

Suppliers and Price of difluoro[4-(hydroxy-kappaO)-4-phenylbut-3-en-2-onato-kappaO]boron

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of difluoro[4-(hydroxy-kappaO)-4-phenylbut-3-en-2-onato-kappaO]boron

Chemical Property:

Vapor Pressure:0.000184mmHg at 25°C
Boiling Point:315.5°Cat760mmHg
Flash Point:133.7°C
Density:g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:210.0663660
Heavy Atom Count:15
Complexity:307

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:[B-]1(OC(=CC(=[O+]1)C2=CC=CC=C2)C)(F)F

Technology Process of difluoro[4-(hydroxy-kappaO)-4-phenylbut-3-en-2-onato-kappaO]boron

There total 13 articles about difluoro[4-(hydroxy-kappaO)-4-phenylbut-3-en-2-onato-kappaO]boron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 63947-74-0
C₁₁H₁₁BF₂O₃

: 917-54-4
methyllithium

: 34075-91-7,14871-98-8
benzoylacetonatoboron difluoride

Guidance literature:: In tetrahydrofuran; at -78 ℃; chemoselective reaction; Inert atmosphere;
DOI:10.1021/ol100620j

Reference yield: 95.0%

: 109-63-7
trifluoroborane diethyl ether

: 93-91-4
1-phenylbutan-1,3-dione

: 34075-91-7,14871-98-8
benzoylacetonatoboron difluoride

Guidance literature:: In benzene; ligand reacted with BF3*(CH2CH3)2O in benzene according to V. M. Neplyevand T. A. Sinenko, Zh. Org. Khim., 1980, 16, 2558 (J. Org. Chem. USSR, 1980, 16 (Engl. Trans.));
DOI:10.1007/s11172-007-0243-5