Diazene, [1,1'-biphenyl]-2-ylphenyl-

Base Information

Chemical Name:Diazene, [1,1'-biphenyl]-2-ylphenyl-
CAS No.:14336-17-5
Molecular Formula:C18H14N2
Molecular Weight:258.323
Hs Code.:
DSSTox Substance ID:DTXSID10482217
Nikkaji Number:J478.955E

Synonyms:Diazene, [1,1'-biphenyl]-2-ylphenyl-;14336-17-5;SCHEMBL3270828;SCHEMBL17707295;DTXSID10482217

Suppliers and Price of Diazene, [1,1'-biphenyl]-2-ylphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Diazene, [1,1'-biphenyl]-2-ylphenyl-

Chemical Property:

XLogP3:5.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:258.115698455
Heavy Atom Count:20
Complexity:301

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=CC=CC=C2N=NC3=CC=CC=C3

Technology Process of Diazene, [1,1'-biphenyl]-2-ylphenyl-

There total 12 articles about Diazene, [1,1'-biphenyl]-2-ylphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 17082-12-1
trans-azobenzene

: 94-36-0
dibenzoyl peroxide

: 14336-17-5
(E)-1-([1,1’-biphenyl]-2-yl)-2-phenyldiazene

Guidance literature:: With palladium diacetate; In chlorobenzene; acetonitrile; at 130 ℃; for 24h; Reagent/catalyst; Solvent; regioselective reaction; Sealed tube;
DOI:10.1039/c4ob00993b

Reference yield: 72.0%

: 100-63-0
phenylhydrazine

: 17082-12-1
trans-azobenzene

: 14336-17-5
(E)-1-([1,1’-biphenyl]-2-yl)-2-phenyldiazene

Guidance literature:: With oxygen; palladium diacetate; In acetonitrile; at 60 ℃; for 24h; Reagent/catalyst; Solvent; Temperature; Catalytic behavior; Sealed tube;
DOI:10.1002/cctc.201500575

Reference yield: 53.0%

: 108-86-1,52753-63-6
bromobenzene

: 17082-12-1
trans-azobenzene

: 14336-17-5
(E)-1-([1,1’-biphenyl]-2-yl)-2-phenyldiazene

Guidance literature:: With [RhCl₂(p-cymene)]2; mesitylenecarboxylic acid; potassium carbonate; In 1,4-dioxane; at 120 ℃; for 18h; Inert atmosphere;