4-[(2-methoxyphenyl)(3-methyl-5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-4-yl)methyl]-5-methyl-2-phenyl-2,4-dihydro-3H-pyrazol-3-one

Base Information

Chemical Name:4-[(2-methoxyphenyl)(3-methyl-5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-4-yl)methyl]-5-methyl-2-phenyl-2,4-dihydro-3H-pyrazol-3-one
CAS No.:143699-01-8
Molecular Formula:C28H26N4O3
Molecular Weight:0.00000
Hs Code.:
Mol file:143699-01-8.mol

Synonyms:

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Chemical Property of 4-[(2-methoxyphenyl)(3-methyl-5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-4-yl)methyl]-5-methyl-2-phenyl-2,4-dihydro-3H-pyrazol-3-one

Chemical Property:

PSA：0.00000
LogP:0.00000

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Technology Process of 4-[(2-methoxyphenyl)(3-methyl-5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-4-yl)methyl]-5-methyl-2-phenyl-2,4-dihydro-3H-pyrazol-3-one

There total 3 articles about 4-[(2-methoxyphenyl)(3-methyl-5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-4-yl)methyl]-5-methyl-2-phenyl-2,4-dihydro-3H-pyrazol-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 135-02-4
ortho-anisaldehyde

: 89-25-8
edaravone

: 143699-01-8
4,4′-[(2-methoxyphenyl)methylene]-bis(3-methyl-1-phenyl-1H-pyrazol-5-ol)

Guidance literature:: With sodium acetate; In ethanol; water; at 20 ℃;
DOI:10.3390/molecules26164960

Reference yield: 92.0%

: 141-97-9
ethyl acetoacetate

: 100-63-0
phenylhydrazine

: 135-02-4
ortho-anisaldehyde

: 143699-01-8
4,4′-[(2-methoxyphenyl)methylene]-bis(3-methyl-1-phenyl-1H-pyrazol-5-ol)

Guidance literature:: With triethylamine sulfate; In neat (no solvent); at 90 ℃; for 0.75h;
DOI:10.4067/S0717-97072015000300003

Reference yield:

: 100-63-0
phenylhydrazine

: 143699-01-8
4,4′-[(2-methoxyphenyl)methylene]-bis(3-methyl-1-phenyl-1H-pyrazol-5-ol)

Guidance literature:: Multi-step reaction with 2 steps

1: 1-methyl-3-(trimethoxysilylpropyl)-imidazoliumhydrogen sulfate supported on sodium montmorillonite / neat (no solvent) / 0.02 h / 100 °C

2: 1-methyl-3-(trimethoxysilylpropyl)-imidazoliumhydrogen sulfate supported on sodium montmorillonite / neat (no solvent) / 0.5 h / 100 °C

With 1-methyl-3-(trimethoxysilylpropyl)-imidazoliumhydrogen sulfate supported on sodium montmorillonite; In neat (no solvent);
DOI:10.1016/j.molliq.2015.04.027