3-(2,4-Dichlorophenyl)-4-hydroxy-1-oxaspiro(4,5)dec-3-en-2-one

Base Information

Chemical Name:3-(2,4-Dichlorophenyl)-4-hydroxy-1-oxaspiro(4,5)dec-3-en-2-one
CAS No.:148476-22-6
Molecular Formula:C15H14Cl2O3
Molecular Weight:313.18
Hs Code.:
Mol file:148476-22-6.mol

Synonyms:1-Oxaspiro[4.5]dec-3-en-2-one,3-(2,4-dichlorophenyl)-4-hydroxy;

Suppliers and Price of 3-(2,4-Dichlorophenyl)-4-hydroxy-1-oxaspiro(4,5)dec-3-en-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
O-Des-(2,2-methylbutyryl)Spirodiclofen
20mg
$ 70.00

Total 31 raw suppliers

Chemical Property of 3-(2,4-Dichlorophenyl)-4-hydroxy-1-oxaspiro(4,5)dec-3-en-2-one

Chemical Property:

Vapor Pressure:4.47E-11mmHg at 25°C
Melting Point:approximate 255℃ (dec.)
Boiling Point:506.4oC at 760 mmHg
PKA:4.50±1.00(Predicted)
Flash Point:260oC
PSA：46.53000
Density:1.44g/cm3
LogP:4.52220

Purity/Quality:

99% ^*data from raw suppliers

O-Des-(2,2-methylbutyryl)Spirodiclofen ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses O-Des-(2,2-methylbutyryl) Spirodiclofen is a metabolite of Spirodiclofen (S682990) in animals and plants. Spirodiclofen is a tetronic acid acaricide used in controlling red mites.

Technology Process of 3-(2,4-Dichlorophenyl)-4-hydroxy-1-oxaspiro(4,5)dec-3-en-2-one

There total 14 articles about 3-(2,4-Dichlorophenyl)-4-hydroxy-1-oxaspiro(4,5)dec-3-en-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.7%

: 1127-01-1
ethyl 1-hydroxycyclohexanecarboxylate

: 53056-20-5
2,4-dichlorophenylacetyl chloride

: 148476-22-6
3-(2,4-dichlorophenyl)-4-hydroxy-1-oxaspiro[4.5]dec-3-en-2-one

Guidance literature:: ethyl 1-hydroxycyclohexanecarboxylate; 2,4-dichlorophenylacetyl chloride; With dmap; at 100 ℃; for 6h;

With potassium hydroxide; In N,N-dimethyl-formamide; at 50 ℃; for 3h;

Reference yield: 85.6%

: C₁₆H₁₈Cl₂O₄

: 148476-22-6
3-(2,4-dichlorophenyl)-4-hydroxy-1-oxaspiro[4.5]dec-3-en-2-one

Guidance literature:: With potassium tert-butylate; In ethanol; for 8h; Reflux;
DOI:10.1134/S1068162021010295

Reference yield: 83.5%

: 19719-28-9
2,4-dichlorophenylacetic acid

: 1127-01-1
ethyl 1-hydroxycyclohexanecarboxylate

: 148476-22-6
3-(2,4-dichlorophenyl)-4-hydroxy-1-oxaspiro[4.5]dec-3-en-2-one

Guidance literature:: 2,4-dichlorophenylacetic acid; ethyl 1-hydroxycyclohexanecarboxylate; With trichlorophosphate; In toluene; at 20 ℃;

With sodium hydroxide; for 6h; Reflux;