1,2-Phenanthrenediol, 1,2,3,4-tetrahydro-, diacetate, trans-

Base Information

Chemical Name:1,2-Phenanthrenediol, 1,2,3,4-tetrahydro-, diacetate, trans-
CAS No.:60967-93-3
Molecular Formula:C18H18O4
Molecular Weight:298.3331
Hs Code.:
DSSTox Substance ID:DTXSID40209813
Wikidata:Q83084270

Synonyms:1,2-Phenanthrenediol, 1,2,3,4-tetrahydro-, diacetate, trans-;60967-93-3;1,2,3,4-Tetrahydro-1,2-phenanthrenediol diacetate, trans-;DTXSID40209813

Suppliers and Price of 1,2-Phenanthrenediol, 1,2,3,4-tetrahydro-, diacetate, trans-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Phenanthrenediol, 1,2,3,4-tetrahydro-, diacetate, trans-

Chemical Property:

Vapor Pressure:1.18E-07mmHg at 25°C
Boiling Point:431.6°Cat760mmHg
Flash Point:216.3°C
Density:1.22g/cm³
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:298.12050905
Heavy Atom Count:22
Complexity:433

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OC1CCC2=C(C1OC(=O)C)C=CC3=CC=CC=C23
Isomeric SMILES:CC(=O)O[C@@H]1CCC2=C([C@H]1OC(=O)C)C=CC3=CC=CC=C23

Technology Process of 1,2-Phenanthrenediol, 1,2,3,4-tetrahydro-, diacetate, trans-

There total 2 articles about 1,2-Phenanthrenediol, 1,2,3,4-tetrahydro-, diacetate, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60890-34-8,60890-35-9,64069-84-7,64069-87-0
(1R)-trans-1,2-diacetoxy-1,2-dihydro-phenanthrene

: 60967-93-3,64069-85-8,64069-88-1
(1R)-trans-1,2-diacetoxy-1,2,3,4-tetrahydro-phenanthrene

Guidance literature:: With ethanol; platinum; Hydrogenation;

Reference yield:

: 38399-10-9
3,4-dihydrophenanthrene

: 563-63-3
silver(I) acetate

: 60967-93-3,64069-85-8,64069-88-1
(+/-)-trans-1,2-diacetoxy-1,2,3,4-tetrahydro-phenanthrene

Guidance literature:: With iodine;
DOI:10.1021/jo00424a036

Reference yield:

: 60967-93-3,64069-85-8,64069-88-1
(+/-)-trans-1,2-diacetoxy-1,2,3,4-tetrahydro-phenanthrene

: 60917-41-1,28622-66-4
trans-1,2-dihydroxy-1,2-dihydrophenanthrene

Guidance literature:: Multi-step reaction with 3 steps

1: NBS, AIBN

2: NaHCO₃

3: NH₃ / methanol

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); ammonia; sodium hydrogencarbonate; In methanol;
DOI:10.1021/jo00424a036