H2dcbpb

Base Information

Chemical Name:H2dcbpb
CAS No.:166897-61-6
Molecular Formula:C₂₆H₂₈Cl₂N₄O₂
Molecular Weight:499.44
Hs Code.:
DSSTox Substance ID:DTXSID201133078
Nikkaji Number:J667.077F

Synonyms:H2dcbpb;SCHEMBL5697335;DTXSID201133078;1,2-bis(4-tert-butyl-pyridine-2-carboxamido)-4,5-dichlorobenzene;N,N'-(4,5-Dichloro-1,2-phenylene)bis(4-tert-butyl-2-pyridinecarboxamide);2-Pyridinecarboxamide, N,N'-(4,5-dichloro-1,2-phenylene)bis[4-(1,1-dimethylethyl)-];N,N'-(4,5-Dichloro-1,2-phenylene)bis[4-(1,1-dimethylethyl)-2-pyridinecarboxamide];166897-61-6;4-tert-butyl-N-[2-[(4-tert-butylpyridine-2-carbonyl)amino]-4,5-dichloro-phenyl]pyridine-2-carboxamide

Suppliers and Price of H2dcbpb

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of H2dcbpb

Chemical Property:

XLogP3:6.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:498.1589315
Heavy Atom Count:34
Complexity:661

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C1=CC(=NC=C1)C(=O)NC2=CC(=C(C=C2NC(=O)C3=NC=CC(=C3)C(C)(C)C)Cl)Cl

Technology Process of H2dcbpb

There total 2 articles about H2dcbpb which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23569-17-7
4-tert-butylpyridine N-oxide

: 166897-61-6
N,N'-(4,5-dichloro-o-phenylene)bis(4-tert-butylpyridine-2-carboxamide)

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) dimethyl sulfate / 1.) 95 deg C, 3 h, 2.) H₂O, r.t., 6 h

2: aq. HCl / 24 h / Heating

3: triphenyl phosphite / pyridine / 2 h / Heating

With triphenyl phosphite; hydrogenchloride; dimethyl sulfate; In pyridine;
DOI:10.1039/DT9950002215

Reference yield:

: 42205-73-2
4-tert-butyl-2-cyanopyridine

: 166897-61-6
N,N'-(4,5-dichloro-o-phenylene)bis(4-tert-butylpyridine-2-carboxamide)

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl / 24 h / Heating

2: triphenyl phosphite / pyridine / 2 h / Heating

With triphenyl phosphite; hydrogenchloride; In pyridine;
DOI:10.1039/DT9950002215

Reference yield: 30.0%

: 15529-49-4,41756-81-4
tris(triphenylphosphine)ruthenium(II) chloride

: 166897-61-6
N,N'-(4,5-dichloro-o-phenylene)bis(4-tert-butylpyridine-2-carboxamide)

: 166897-60-5
Ru(C₆H₂Cl₂(NCOC₅H₃NC(CH₃)3)2)(P(C₆H₅)3)Cl

Guidance literature:: With O₂; Et₃N; In ethanol; refluxing (O2-stream, 12 h); evapn., extn. (CH2Cl2), evapn., recrystn. (CH2Cl2/Et2O); elem. anal.;
DOI:10.1039/DT9950002215