Uridine, 2'-O-[(methylthio)methyl]-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disil oxanediyl]-

Base Information

Chemical Name:Uridine, 2'-O-[(methylthio)methyl]-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disil oxanediyl]-
CAS No.:174497-93-9
Molecular Formula:C23H42N2O7SSi2
Molecular Weight:546.833
Hs Code.:

Synonyms:

Suppliers and Price of Uridine, 2'-O-[(methylthio)methyl]-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disil oxanediyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 2 raw suppliers

Chemical Property of Uridine, 2'-O-[(methylthio)methyl]-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disil oxanediyl]-

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Uridine, 2'-O-[(methylthio)methyl]-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disil oxanediyl]-

There total 2 articles about Uridine, 2'-O-[(methylthio)methyl]-3',5'-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disil oxanediyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 4756-05-2
thioacetone

: 69304-38-7
3',5'-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

: 174497-93-9
2'-O-methylthiomethyl-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

Guidance literature:: With acetic anhydride; In acetic acid;

Reference yield: 20.0%

: 75-18-3
dimethylsulfide

: 69304-38-7
3',5'-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

: 84828-97-7
1-((6aR,8R,9aR)-2,2,4,4-tetraisopropyl-9-oxotetrahydro-6H-furo[3,2-f][1,3,5,2,4]trioxadisilocin-8-yl)pyrimidine-2,4(1H,3H)-dione

: 174497-93-9
2'-O-methylthiomethyl-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; acetonitrile;
DOI:10.1080/07328319708006114

Reference yield: 66.0%

: 174497-93-9
2'-O-methylthiomethyl-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

: 2,5-dimethoxy-4-nitro-1-hydroxymethylbenzene

: C₁₉H₂₃N₃O₁₁

Guidance literature:: 2'-O-methylthiomethyl-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine; 2,5-dimethoxy-4-nitro-1-hydroxymethylbenzene; With pyridine; N-iodo-succinimide; trifluorormethanesulfonic acid; In tetrahydrofuran; toluene; at -40 ℃; for 2h; Inert atmosphere; Molecular sieve;

With methanol; ammonium fluoride; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/acs.orglett.0c02086