Silane, (4-bromo-2-methylphenoxy)(1,1-dimethylethyl)dimethyl-

Base Information

Chemical Name:Silane, (4-bromo-2-methylphenoxy)(1,1-dimethylethyl)dimethyl-
CAS No.:179636-73-8
Molecular Formula:C13H21BrOSi
Molecular Weight:301.299
Hs Code.:
Mol file:179636-73-8.mol

Synonyms:3-bromo-6-tert-butyldimethylsiloxytoluene;2-(t-butyldimethylsilyloxy)-5-bromotoluene;(4-Bromo-2-methyl-phenoxy)-tert-butyl-dimethyl-silane;(4-bromo-2-methylphenoxy)(tert-butyl)dimethylsilane;3-bromo-6-tetrt-butyldimethylsiloxytoluene;4-tert-butyldimethylsilyloxy-3-methylbromobenzene;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, (4-bromo-2-methylphenoxy)(1,1-dimethylethyl)dimethyl-

Chemical Property:

PSA：9.23000
LogP:5.14150

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Silane, (4-bromo-2-methylphenoxy)(1,1-dimethylethyl)dimethyl-

There total 2 articles about Silane, (4-bromo-2-methylphenoxy)(1,1-dimethylethyl)dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2362-12-1
4-Bromo-2-methylphenol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 179636-73-8
(4-bromo-2-methylphenoxy)(tertiary-butyl)dimethylsilane

Guidance literature:: With dmap; In toluene; at 20 - 25 ℃;
DOI:10.1021/op8002294

Reference yield: 100.0%

: 62790-79-8
2-(tert-butyldimethylsilyloxy)toluene

: 179636-73-8
(4-bromo-2-methylphenoxy)(tertiary-butyl)dimethylsilane

Guidance literature:: With ammonium metavanadate; aluminum tri-bromide; oxygen; In diethyl ether; at 20 ℃; for 8h;
DOI:10.1016/j.tet.2010.06.042

Reference yield: 72.0%

: 179636-73-8
(4-bromo-2-methylphenoxy)(tertiary-butyl)dimethylsilane

: 96-22-0
pentan-3-one

: 633337-85-6
3'-[4-(t-butyldimethylsilyloxy)-3-methylphenyl]pentan-3-ol

Guidance literature:: (4-bromo-2-methylphenoxy)(tertiary-butyl)dimethylsilane; With iodine; magnesium; In tetrahydrofuran; at 90 ℃; for 2.5h;

pentan-3-one; In tetrahydrofuran; at 0 - 50 ℃; for 3h;