2-(3-Methylbut-3-en-1-yl)phenol

Base Information

Chemical Name:2-(3-Methylbut-3-en-1-yl)phenol
CAS No.:18272-65-6
Molecular Formula:C11H14O
Molecular Weight:162.232
Hs Code.:
DSSTox Substance ID:DTXSID90498710
Mol file:18272-65-6.mol

Synonyms:2-(3-Methylbut-3-en-1-yl)phenol;18272-65-6;2-(3-methylbut-3-enyl)phenol;Phenol, 2-(3-methyl-3-buten-1-yl)-;o-isopentenylphenol;SCHEMBL5380034;DTXSID90498710;A933973

Suppliers and Price of 2-(3-Methylbut-3-en-1-yl)phenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-(3-Methylbut-3-en-1-yl)phenol

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:162.104465066
Heavy Atom Count:12
Complexity:151

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=C)CCC1=CC=CC=C1O

Technology Process of 2-(3-Methylbut-3-en-1-yl)phenol

There total 17 articles about 2-(3-Methylbut-3-en-1-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 18272-85-0
4-(2-methoxyphenyl)-2-methyl-1-butene

: 18272-65-6
4-(2-hydroxyphenyl)-2-methyl-1-butene

Guidance literature:: With sodium hydride; ethanethiol; In N,N-dimethyl-formamide; mineral oil; for 3h; Reflux;
DOI:10.1021/jacs.8b02607

Reference yield: 35.0%

: 95-48-7,77504-84-8
ortho-cresol

: 563-47-3
3-Chloro-2-methylpropene

: 18272-65-6
4-(2-hydroxyphenyl)-2-methyl-1-butene

Guidance literature:: ortho-cresol; With n-butyllithium; potassium tert-butylate; In hexane; n-heptane; for 3h; Inert atmosphere; Reflux;

3-Chloro-2-methylpropene; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; water; Inert atmosphere;
DOI:10.1021/ol9027286

Reference yield:

: 52289-93-7
o-Methoxybenzyl bromide

: 18272-65-6
4-(2-hydroxyphenyl)-2-methyl-1-butene

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium / Inert atmosphere

2: sodium thioethylate / N,N-dimethyl-formamide / Reflux; Inert atmosphere

With magnesium; sodium thioethylate; In N,N-dimethyl-formamide;
DOI:10.1002/anie.201600379