L-Valinamide, N-cyclopropylglycyl-N-[(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(2-meth ylpropyl)amino]-2-hydroxy-1-(phenylmethyl)propyl]-3-methyl-

Base Information

Chemical Name:L-Valinamide, N-cyclopropylglycyl-N-[(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(2-meth ylpropyl)amino]-2-hydroxy-1-(phenylmethyl)propyl]-3-methyl-
CAS No.:183812-77-3
Molecular Formula:C32H46N4O7S
Molecular Weight:630.806
Hs Code.:
Mol file:183812-77-3.mol

L-Valinamide,
N-cyclopropylglycyl-N-[(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(2-meth
ylpropyl)amino]-2-hydroxy-1-(phenylmethyl)propyl]-3-methyl-

Synonyms:

Suppliers and Price of L-Valinamide, N-cyclopropylglycyl-N-[(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(2-meth ylpropyl)amino]-2-hydroxy-1-(phenylmethyl)propyl]-3-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of L-Valinamide, N-cyclopropylglycyl-N-[(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(2-meth ylpropyl)amino]-2-hydroxy-1-(phenylmethyl)propyl]-3-methyl-

Chemical Property:

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of L-Valinamide, N-cyclopropylglycyl-N-[(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(2-meth ylpropyl)amino]-2-hydroxy-1-(phenylmethyl)propyl]-3-methyl-

There total 3 articles about L-Valinamide, N-cyclopropylglycyl-N-[(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(2-meth ylpropyl)amino]-2-hydroxy-1-(phenylmethyl)propyl]-3-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 183553-81-3
N-[2R-hydroxy-3-[[(1,3-benzodioxol-5-yl) sulfonyl](2-methylpropyl)amino]-1S-(phenylmethyl)propyl]-2S-[(chloroacetyl)amino]-3,3-dimethylbutanamide

: 765-30-0
Cyclopropylamine

: 183812-77-3
DMP 853

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 24h;

Reference yield:

: 565227-88-5
tert-butyl 2-{(1S)-1-[({(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(isobutyl)amino]-1-benzyl-2-hydroxypropyl}amino)carbonyl]-2,2-dimethylpropyl}amino-2-oxoethyl(cyclopropyl) carbamate

: 183812-77-3
DMP 853

Guidance literature:: With trifluoroacetic acid; In dichloromethane;
DOI:10.1002/jlcr.676

Reference yield:

: 565227-89-6
tert-butyl 2-{(1S)-1-[({(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(isobutyl)amino]-1-benzyl-2-oxopropyl}amino)carbonyl]-2,2-dimethylpropyl}amino-2-oxoethyl(cyclopropyl) carbamate

: 183812-77-3
DMP 853

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / NaBH₄ / ethanol / 20 °C

2: TFA / CH₂Cl₂

With sodium tetrahydroborate; trifluoroacetic acid; In ethanol; dichloromethane;
DOI:10.1002/jlcr.676