tert-butyl 2-{(1S)-1-[({(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(isobutyl)amino]-1-benzyl-2-hydroxy-2-[3H]-propyl}amino)carbonyl]-2,2-dimethylpropyl}amino-2-oxoethyl(cyclopropyl) carbamate

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Chemical Name:tert-butyl 2-{(1S)-1-[({(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(isobutyl)amino]-1-benzyl-2-hydroxy-2-[3H]-propyl}amino)carbonyl]-2,2-dimethylpropyl}amino-2-oxoethyl(cyclopropyl) carbamate
CAS No.:565227-90-9
Molecular Formula:C₃₇H₅₄N₄O₉S
Molecular Weight:732.915
Hs Code.:

tert-butyl 2-{(1S)-1-[({(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(isobutyl)amino]-1-benzyl-2-hydroxy-2-[3H]-propyl}amino)carbonyl]-2,2-dimethylpropyl}amino-2-oxoethyl(cyclopropyl) carbamate

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Chemical Property of tert-butyl 2-{(1S)-1-[({(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(isobutyl)amino]-1-benzyl-2-hydroxy-2-[3H]-propyl}amino)carbonyl]-2,2-dimethylpropyl}amino-2-oxoethyl(cyclopropyl) carbamate

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Technology Process of tert-butyl 2-{(1S)-1-[({(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(isobutyl)amino]-1-benzyl-2-hydroxy-2-[3H]-propyl}amino)carbonyl]-2,2-dimethylpropyl}amino-2-oxoethyl(cyclopropyl) carbamate

There total 4 articles about tert-butyl 2-{(1S)-1-[({(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(isobutyl)amino]-1-benzyl-2-hydroxy-2-[3H]-propyl}amino)carbonyl]-2,2-dimethylpropyl}amino-2-oxoethyl(cyclopropyl) carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 565227-89-6
tert-butyl 2-{(1S)-1-[({(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(isobutyl)amino]-1-benzyl-2-oxopropyl}amino)carbonyl]-2,2-dimethylpropyl}amino-2-oxoethyl(cyclopropyl) carbamate

: C₃₇H₅₃⁽³⁾HN₄O₉S

: C₃₇H₅₃⁽³⁾HN₄O₉S

: 565227-90-9
tert-butyl 2-{(1S)-1-[({(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(isobutyl)amino]-1-benzyl-2-hydroxy-2-[3H]-propyl}amino)carbonyl]-2,2-dimethylpropyl}amino-2-oxoethyl(cyclopropyl) carbamate

: C₃₇H₅₃⁽³⁾HN₄O₉S

Guidance literature:: With sodium boron [ 3H]hydride; In ethanol; at 20 ℃; for 4h;
DOI:10.1002/jlcr.676

Reference yield:

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 565227-90-9
tert-butyl 2-{(1S)-1-[({(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(isobutyl)amino]-1-benzyl-2-hydroxy-2-[3H]-propyl}amino)carbonyl]-2,2-dimethylpropyl}amino-2-oxoethyl(cyclopropyl) carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / triethylamine / H₂O; dioxane / 4 h / 20 °C

2: 90 percent / oxalyl chloride; DMSO; triethylamine / CH₂Cl₂ / -78 - 20 °C

3: sodium borotritide / ethanol / 4 h / 20 °C

With oxalyl dichloride; sodium boron [ 3H]hydride; dimethyl sulfoxide; triethylamine; In 1,4-dioxane; ethanol; dichloromethane; water; 2: Swern oxidation;
DOI:10.1002/jlcr.676

Reference yield:

: 183812-77-3
DMP 853

: 565227-90-9
tert-butyl 2-{(1S)-1-[({(1S,2R)-3-[(1,3-benzodioxol-5-ylsulfonyl)(isobutyl)amino]-1-benzyl-2-hydroxy-2-[3H]-propyl}amino)carbonyl]-2,2-dimethylpropyl}amino-2-oxoethyl(cyclopropyl) carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / triethylamine / H₂O; dioxane / 4 h / 20 °C

2: 90 percent / oxalyl chloride; DMSO; triethylamine / CH₂Cl₂ / -78 - 20 °C

3: sodium borotritide / ethanol / 4 h / 20 °C

With oxalyl dichloride; sodium boron [ 3H]hydride; dimethyl sulfoxide; triethylamine; In 1,4-dioxane; ethanol; dichloromethane; water; 2: Swern oxidation;
DOI:10.1002/jlcr.676