4-Ethoxy-3-iodobenzaldehyde

Base Information

Chemical Name:4-Ethoxy-3-iodobenzaldehyde
CAS No.:184033-45-2
Molecular Formula:C9H9IO2
Molecular Weight:276.07100
Hs Code.:2913000090
DSSTox Substance ID:DTXSID00397361
Wikidata:Q82198635
Mol file:184033-45-2.mol

Synonyms:4-ethoxy-3-iodobenzaldehyde;184033-45-2;CHEMBRDG-BB 6448120;DTXSID00397361;MFCD02629428;STL371696;AKOS002341020;4-Ethoxy-3-iodobenzaldehyde, AldrichCPR

Suppliers and Price of 4-Ethoxy-3-iodobenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-ETHOXY-3-IODOBENZALDEHYDE 95.00%
250MG
$ 659.74

Total 3 raw suppliers

Chemical Property of 4-Ethoxy-3-iodobenzaldehyde

Chemical Property:

Vapor Pressure:0.000111mmHg at 25°C
Boiling Point:336.6oC at 760 mmHg
Flash Point:157.4oC
PSA：26.30000
Density:1.686g/cm3
LogP:2.50240
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:275.96473
Heavy Atom Count:12
Complexity:150

Purity/Quality:

95% ^*data from raw suppliers

4-ETHOXY-3-IODOBENZALDEHYDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 41
Safety Statements: 26-39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC1=C(C=C(C=C1)C=O)I

Technology Process of 4-Ethoxy-3-iodobenzaldehyde

There total 3 articles about 4-Ethoxy-3-iodobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 10031-82-0
4-ethoxybenzaldehyde

: 184033-45-2
3-iodo-4-ethoxybenzaldehyde

Guidance literature:: With iron(III) chloride; N-iodo-succinimide; 1-butyl-3-methylimidazolium trifluoromethanesulfonimide; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/acs.orglett.5b02345

Reference yield:

: 60032-63-5
4-hydroxy-3-iodo-benzaldehyde

: 75-03-6
ethyl iodide

: 184033-45-2
3-iodo-4-ethoxybenzaldehyde

Guidance literature:: With potassium carbonate; In acetone; for 30h; Ambient temperature;
DOI:10.1021/jm9602672

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 184033-45-2
3-iodo-4-ethoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1.8 g / ICl, AcOH / CH₂Cl₂ / 17 h / Ambient temperature

2: 0.45 g / K₂CO₃ / acetone / 30 h / Ambient temperature

With Iodine monochloride; potassium carbonate; acetic acid; In dichloromethane; acetone;
DOI:10.1021/jm9602672