3-Phenylcarbazic acid 2-chloroethyl ester

Base Information

• Chemical Name: 3-Phenylcarbazic acid 2-chloroethyl ester
• CAS No.: 5923-43-3
• Molecular Formula: C9H11ClN2O2
• Molecular Weight: 214.652
• Hs Code.: 2928000090
• NSC Number: 43645
• DSSTox Substance ID: DTXSID80207974
• Nikkaji Number: J48.441E
• Wikidata: Q83082014
• Mol file: 5923-43-3.mol

Synonyms:3-Phenylcarbazic acid 2-chloroethyl ester;5923-43-3;2-Chloroethyl N(sup2)-phenylcarbazate;2-Chloroethyl N(sup 2)-phenylcarbazate;NSC 43645;BRN 0646470;CARBAZIC ACID, 3-PHENYL-, 2-CHLOROETHYL ESTER;2-15-00-00106 (Beilstein Handbook Reference);WLN: G2OVMMR;DTXSID80207974;2-chloroethyl N-(anilino)carbamate;Carbazic acid, 2-chloroethyl ester;NSC43645;NSC-43645;2-chloroethyl 2-phenylhydrazinecarboxylate;LS-51660;Hydrazinecarboxylic acid, 2-phenyl-, 2-chloroethyl ester

Chemical Property of 3-Phenylcarbazic acid 2-chloroethyl ester

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 50.36000
• Density: 1.296g/cm³
• LogP: 2.44240
• XLogP3: 1.4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 214.0509053
• Heavy Atom Count: 14
• Complexity: 172

Purity/Quality:

2-CHLOROETHYL 2-PHENYLHYDRAZINECARBOXYLATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)NNC(=O)OCCCl

Technology Process of 3-Phenylcarbazic acid 2-chloroethyl ester

There total 1 articles about 3-Phenylcarbazic acid 2-chloroethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Chloroethyl chloroformate (627-11-2) + phenylhydrazine (100-63-0) → 3-phenyl-carbazic acid-(2-chloro-ethyl ester) (5923-43-3)

Guidance literature:

With pyridine; water;

Reference yield:

3-phenyl-carbazic acid-(2-chloro-ethyl ester) (5923-43-3) → phenylhydrazine (100-63-0) + 2-chloro-ethanol (107-07-3)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; at 25 ℃; Rate constant;

upstream raw materials:

2-Chloroethyl chloroformate

phenylhydrazine

Downstream raw materials:

phenylhydrazine

2-chloro-ethanol