(3-Bromophenyl)triphenylsilane

Base Information

• Chemical Name: (3-Bromophenyl)triphenylsilane
• CAS No.: 185626-73-7
• Molecular Formula: C24H19BrSi
• Molecular Weight: 415.404
• Mol file: 185626-73-7.mol

Synonyms:(3-bromophenyl)triphenylsilane;Silane, (3-bromophenyl)triphenyl-;3-bromophenyltriphenylsilane;

Chemical Property of (3-Bromophenyl)triphenylsilane

Chemical Property:

• Melting Point: 135.0 to 139.0 °C
• Boiling Point: 469.9±37.0 °C(Predicted)
• PSA: 0.00000
• Density: 1.30±0.1 g/cm3(Predicted)
• LogP: 3.82650
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

(3-Bromophenyl)triphenylsilane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3-Bromophenyl)triphenylsilane

There total 1 articles about (3-Bromophenyl)triphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Triphenylsilyl chloride (76-86-8) + 1,3-dibromobenzene (108-36-1) → 3-bromophenyltriphenylsilyl chloride (185626-73-7)

Guidance literature:

1,3-dibromobenzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h;

Triphenylsilyl chloride; In tetrahydrofuran; at 20 ℃; for 12h;

Reference yield: 83.0%

3-bromophenyltriphenylsilyl chloride (185626-73-7) + 4,6-diphenyl-2-[5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,1': 2',1-terphenyl-3-yl]-1,3,5-triazine → 2,4-diphenyl-6-[3-triphenylsilyl-1,1':5',1'':2'',1'''-quaterphenyl-3'-yl]-1,3,5-triazine

Guidance literature:

With palladium diacetate; potassium carbonate; XPhos; In tetrahydrofuran; water; for 24h; Inert atmosphere; Reflux;

Reference yield: 81.0%

3-bromophenyltriphenylsilyl chloride (185626-73-7) + bis(pinacol)diborane (73183-34-3) → triphenyl [3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]silane (1391041-75-0)

Guidance literature:

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; at 60 - 80 ℃; for 14h; Inert atmosphere;

upstream raw materials:

Triphenylsilyl chloride

1,3-dibromobenzene

Downstream raw materials:

C₄₄H₃₁N₃SSi

B-[3-(triphenylsilyl)phenyl]-boronic acid

C₂₈H₂₁ClN₂Si

C₄₀H₂₉N₃Si

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