Germane, triethyl(phenylmethyl)-

Base Information

Chemical Name:Germane, triethyl(phenylmethyl)-
CAS No.:2945-41-7
Molecular Formula:C13H22 Ge
Molecular Weight:250.908
Hs Code.:
DSSTox Substance ID:DTXSID50183655
Nikkaji Number:J1.345.373J
Wikidata:Q83054475
Mol file:2945-41-7.mol

Synonyms:Germane, triethyl(phenylmethyl)-;2945-41-7;Germane,triethyl(phenylmethyl)-;triethyl(phenylmethyl)germane;DTXSID50183655

Suppliers and Price of Germane, triethyl(phenylmethyl)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Germane, triethyl(phenylmethyl)-

Chemical Property:

Vapor Pressure:0.00743mmHg at 25°C
Boiling Point:277.9°Cat760mmHg
Flash Point:115.8°C
Density:g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:5
Exact Mass:252.0933285
Heavy Atom Count:14
Complexity:135

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC[Ge](CC)(CC)CC1=CC=CC=C1

Technology Process of Germane, triethyl(phenylmethyl)-

There total 6 articles about Germane, triethyl(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1589-82-8
phenylmagnesium bromide

: 1067-10-3
Bromotriethylgermanium

: 2945-41-7
triethylgermylmethylbenzene

Guidance literature:: In diethyl ether; addn. of Et3GeBr soln. to a soln. of benzylmagnesium bromide, refluxingovernight; hydrolyzing (ice, aq. HCl), column chromy. (silica gel, hexane), fractional distn;
DOI:10.1246/bcsj.59.3169

Reference yield: 80.0%

: 100-39-0
benzyl bromide

: 1067-10-3
Bromotriethylgermanium

: 2945-41-7
triethylgermylmethylbenzene

Guidance literature:: With magnesium; In tetrahydrofuran; byproducts: MgBr2; Sonication; the mixt. of magnesium, germane and halogen-compound in THF was sonicated for 2 h (inert atm.); the mixt. was washed with satd. soln. of NaCl, extd. with diethyl ether,the organic layer was dried over MgSO4, the solvent was removed under r educed pressure, column chromy. (petroleum ether-diethyl ether 95/5);
DOI:10.1016/S0022-328X(03)00053-6