p-Cyanobenzal-p-anisidine

Base Information

Chemical Name:p-Cyanobenzal-p-anisidine
CAS No.:20256-89-7
Molecular Formula:C₁₅H₁₂N₂O
Molecular Weight:236.273
Hs Code.:
NSC Number:90302
DSSTox Substance ID:DTXSID30293509
Nikkaji Number:J126.374I
Mol file:20256-89-7.mol

Synonyms:p-Cyanobenzal-p-anisidine;20256-89-7;4-(((4-Methoxyphenyl)imino)methyl)benzonitrile;4-[(4-methoxyphenyl)iminomethyl]benzonitrile;p-Tolunitrile, .alpha.-[(p-methoxyphenyl)imino]-;Benzonitrile, 4-[[(4-methoxyphenyl)imino]methyl]-;N-(4-Cyanobenzylidene)-para-anisidine;4-{[(4-methoxyphenyl)imino]methyl}benzonitrile;NSC90302;SCHEMBL295243;SCHEMBL3181342;DTXSID30293509;ASVSTYQWCPHCFY-GZTJUZNOSA-N;ASVSTYQWCPHCFY-UHFFFAOYSA-N;NSC-90302;AKOS003408208;AKOS024333029;4-[(4-methoxyphenylimino)methyl]benzonitrile;4-((E)-[(4-Methoxyphenyl)imino]methyl)benzonitrile #

Suppliers and Price of p-Cyanobenzal-p-anisidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
N-(4-CYANOBENZYLIDENE)-PARA-ANISIDINE Aldrich
250mg
$ 57.00

Crysdot
4-(((4-Methoxyphenyl)imino)methyl)benzonitrile 95+%
1g
$ 574.00

Crysdot
4-(((4-Methoxyphenyl)imino)methyl)benzonitrile 95+%
5g
$ 1166.00

Alichem
4-(((4-Methoxyphenyl)imino)methyl)benzonitrile
5g
$ 1233.75

Alichem
4-(((4-Methoxyphenyl)imino)methyl)benzonitrile
1g
$ 638.00

Total 8 raw suppliers

Chemical Property of p-Cyanobenzal-p-anisidine

Chemical Property:

Vapor Pressure:3.01E-07mmHg at 25°C
Boiling Point:419.6°Cat760mmHg
Flash Point:207.5°C
PSA：45.38000
Density:1.05g/cm³
LogP:3.31748
Storage Temp.:Sealed in dry,Room Temperature
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:236.094963011
Heavy Atom Count:18
Complexity:315

Purity/Quality:

98%,99%, ^*data from raw suppliers

N-(4-CYANOBENZYLIDENE)-PARA-ANISIDINE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)N=CC2=CC=C(C=C2)C#N

Technology Process of p-Cyanobenzal-p-anisidine

There total 9 articles about p-Cyanobenzal-p-anisidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 5416-93-3
4-Methoxyphenyl isocyanate

: 105-07-7
4-cyanobenzaldehyde

: 114046-25-2,20256-89-7
4-(((4-methoxyphenyl)imino)methyl)benzonitrile

Guidance literature:: 4-Methoxyphenyl isocyanate; 4-cyanobenzaldehyde; With tetrabutoxytitanium; In tetrahydrofuran; at 20 ℃; for 60h; Inert atmosphere;

With water; In tetrahydrofuran; for 1h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2009.10.044

Reference yield: 76.0%

: 104-94-9
4-methoxy-aniline

: 105-07-7
4-cyanobenzaldehyde

: 114046-25-2,20256-89-7
4-(((4-methoxyphenyl)imino)methyl)benzonitrile

: 4-(((4-methoxyphenyl)amino)methyl)benzonitrile

Guidance literature:: With [2,2]bipyridinyl; carbon monoxide; bis[diiodido(η⁶-p-cymene)osmium(II)]; In water; at 120 ℃; for 22h; under 37503.8 Torr;
DOI:10.1039/d1cy00695a

Reference yield: 74.0%

: 104-94-9
4-methoxy-aniline

: 105-07-7
4-cyanobenzaldehyde

: 114046-25-2,20256-89-7
4-(((4-methoxyphenyl)imino)methyl)benzonitrile

Guidance literature:: With p-toluenesulfonic acid on sillica gel; In neat (no solvent); for 2h; Sonication; Green chemistry;
DOI:10.1080/00397911.2018.1540047