Cyclohexanone, 4-(1-phenyl-4-piperidinylidene)-

Base Information

Chemical Name:Cyclohexanone, 4-(1-phenyl-4-piperidinylidene)-
CAS No.:193960-10-0
Molecular Formula:C17H21NO
Molecular Weight:255.35500
Hs Code.:
Mol file:193960-10-0.mol

Synonyms:Cyclohexanone,4-(1-phenyl-4-piperidinylidene);9-(1-Phenylpiperidin-4-ylidene)cyclohexanone;4-(1-phenylpiperidin-4-ylidene)cyclohexanone;

Suppliers and Price of Cyclohexanone, 4-(1-phenyl-4-piperidinylidene)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexanone, 4-(1-phenyl-4-piperidinylidene)-

Chemical Property:

PSA：20.31000
LogP:3.79150

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohexanone, 4-(1-phenyl-4-piperidinylidene)-

There total 4 articles about Cyclohexanone, 4-(1-phenyl-4-piperidinylidene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 299158-68-2
9-(1-Phenylpiperidin-4-ylidene)-3,3-dimethyl-1,5-dioxaspiro[5.5]undecane

: 193960-10-0
9-(1-Phenylpiperidin-4-ylidene)cyclohexanone

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; for 4h; Heating;
DOI:10.1002/1521-3765(20000818)6:16<2948::AID-CHEM2948>3.0.CO;2-0

Reference yield:

: 19125-34-9
1-phenylpiperidin-4-one

: 193960-10-0
9-(1-Phenylpiperidin-4-ylidene)cyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / tetrahydrofuran; hexane / 2 h / 50 °C

1.2: 36 percent / tetrahydrofuran; hexane / 2 h / 50 °C

2.1: 71 percent / N,N-dimethylformamide dineopentyl acetal / acetonitrile / Heating

3.1: 92 percent / aq. HCl / tetrahydrofuran / 4 h / Heating

With hydrogenchloride; N,N-dimethylformamide dineopentyl acetal; lithium diisopropyl amide; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1002/1521-3765(20000818)6:16<2948::AID-CHEM2948>3.0.CO;2-0

Reference yield:

: 169822-66-6
3,3-Dimethyl-1,5-dioxaspiro[5.5]undecane-9-carboxylic acid

: 193960-10-0
9-(1-Phenylpiperidin-4-ylidene)cyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / tetrahydrofuran; hexane / 2 h / 50 °C

1.2: 36 percent / tetrahydrofuran; hexane / 2 h / 50 °C

2.1: 71 percent / N,N-dimethylformamide dineopentyl acetal / acetonitrile / Heating

3.1: 92 percent / aq. HCl / tetrahydrofuran / 4 h / Heating

With hydrogenchloride; N,N-dimethylformamide dineopentyl acetal; lithium diisopropyl amide; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1002/1521-3765(20000818)6:16<2948::AID-CHEM2948>3.0.CO;2-0