n-Propyl trichloroacetate

Base Information

• Chemical Name: n-Propyl trichloroacetate
• CAS No.: 13313-91-2
• Molecular Formula: C5H7 Cl3 O2
• Molecular Weight: 205.468
• Hs Code.: 2915400090
• Mol file: 13313-91-2.mol

Synonyms:Aceticacid, trichloro-, propyl ester (7CI,8CI,9CI); NSC 50958; Propyltrichloroacetate; n-Propyl trichloroacetate

Chemical Property of n-Propyl trichloroacetate

Chemical Property:

• Vapor Pressure: 0.66mmHg at 25°C
• Refractive Index: 1.4501 (estimate)
• Boiling Point: 186.5°Cat760mmHg
• Flash Point: 67.6°C
• PSA: 26.30000
• Density: 1.381g/cm³
• LogP: 2.30980

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of n-Propyl trichloroacetate

There total 4 articles about n-Propyl trichloroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

propan-1-ol (71-23-8) + trichloroacetic acid (76-03-9) → n-propyl trichloroacetate (13313-91-2)

Guidance literature:

DOI:10.1021/ja01857a036

Reference yield:

propan-1-ol (71-23-8) + 1,1,1,3,3,3-hexachloro-propan-2-one (116-16-5) → n-propyl trichloroacetate (13313-91-2)

Guidance literature:

With N,N-dimethyl-formamide; at 55 ℃; for 9h; Product distribution; other times, other temperatures, addition of equimolar amount of 2-propanol;

DOI:10.1021/jo00330a028

Reference yield:

propan-1-ol (71-23-8) + trifluoroacetyl chloride (76-02-8) → n-propyl trichloroacetate (13313-91-2)

Guidance literature:

upstream raw materials:

propan-1-ol

trichloroacetic acid

1,1,1,3,3,3-hexachloro-propan-2-one

trifluoroacetyl chloride

Downstream raw materials:

9H-fluorene-9-carboxylic acid