3,4-Dimethoxybenzoic acid trimethylsilyl ester

Base Information

Chemical Name:3,4-Dimethoxybenzoic acid trimethylsilyl ester
CAS No.:2078-16-2
Molecular Formula:C12H18O4Si
Molecular Weight:254.358
Hs Code.:
Mol file:2078-16-2.mol

Synonyms:3,4-Dimethoxybenzoic acid trimethylsilyl ester;Benzoic acid,3,4-dimethoxy-,trimethylsilyl ester;

Suppliers and Price of 3,4-Dimethoxybenzoic acid trimethylsilyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of 3,4-Dimethoxybenzoic acid trimethylsilyl ester

Chemical Property:

PSA：44.76000
LogP:2.69550

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,4-Dimethoxybenzoic acid trimethylsilyl ester

There total 13 articles about 3,4-Dimethoxybenzoic acid trimethylsilyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 93-07-2
Veratric acid

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 2078-16-2
trimethylsilyl 3,4-dimethoxybenzoate

Guidance literature:: In neat (no solvent); at 20 ℃; for 40h; Green chemistry;
DOI:10.1016/j.tet.2016.08.003

Reference yield:

: 22675-96-3
2-methoxyphenoxy-3',4'-dimethoxyacetophenone

: 2078-16-2
trimethylsilyl 3,4-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / tetrahydrofuran; water / 0.33 h / Reflux

2: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether; water / acetone / 1 h / 25 °C / Green chemistry

3: 25 °C

With sodium tetrahydroborate; diphenylether; Fe(TAML)Li; [bis(acetoxy)iodo]benzene; water; In tetrahydrofuran; water; acetone;
DOI:10.1002/ejoc.201301093

Reference yield:

: 93-03-8
(3,4-dimethoxyphenyl)methanol

: 2078-16-2
trimethylsilyl 3,4-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether; water / acetone / 1 h / 25 °C / Green chemistry

2: 25 °C

With diphenylether; Fe(TAML)Li; [bis(acetoxy)iodo]benzene; water; In acetone;
DOI:10.1002/ejoc.201301093