1-Cyclohex-2-en-1-yl-3-methylurea

Base Information

Chemical Name:1-Cyclohex-2-en-1-yl-3-methylurea
CAS No.:33024-57-6
Molecular Formula:C8H14N2O
Molecular Weight:154.2096
Hs Code.:
NSC Number:132931
DSSTox Substance ID:DTXSID50299801
Nikkaji Number:J1.321.648G

Synonyms:33024-57-6;1-cyclohex-2-en-1-yl-3-methylurea;NSC132931;DTXSID50299801;NSC-132931

Suppliers and Price of 1-Cyclohex-2-en-1-yl-3-methylurea

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-Cyclohex-2-en-1-yl-3-methylurea

Chemical Property:

Vapor Pressure:0.000197mmHg at 25°C
Boiling Point:327.9°Cat760mmHg
Flash Point:149.5°C
Density:1.03g/cm³
XLogP3:0.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:154.110613074
Heavy Atom Count:11
Complexity:166

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CNC(=O)NC1CCCC=C1

Technology Process of 1-Cyclohex-2-en-1-yl-3-methylurea

There total 4 articles about 1-Cyclohex-2-en-1-yl-3-methylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 270063-67-7
1-(2-cyclohexen-1-yl)-4-methyl-2-(2-oxo-2-phenylethyl)-1,2,4-triazolidine-3,5-dione

: 33024-57-6
N-(2-cyclohexen-1-yl)-N'-methylurea

Guidance literature:: With potassium hydroxide; In methanol; water; at 80 ℃; for 18h;
DOI:10.1021/ol000044c

Reference yield:

: 154228-83-8
1-(2-cyclohexen-1-yl)-4-methyl-1,2,4-triazolidine-3,5-dione

: 33024-57-6
N-(2-cyclohexen-1-yl)-N'-methylurea

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / tetrahydrofuran / 3 h / 65 °C

1.2: 81 percent / tetrahydrofuran / 18 h / 65 °C

2.1: 72 percent / KOH / methanol; H₂O / 18 h / 80 °C

With potassium hydroxide; sodium hydride; In tetrahydrofuran; methanol; water; 1.1: Deprotonation / 1.2: Alkylation / 2.1: Hydrolysis;
DOI:10.1021/ol000044c

Reference yield:

: 110-83-8
cyclohexene

: 33024-57-6
N-(2-cyclohexen-1-yl)-N'-methylurea

Guidance literature:: Multi-step reaction with 3 steps

1.1: CH₂Cl₂ / 16 h / 20 °C

2.1: NaH / tetrahydrofuran / 3 h / 65 °C

2.2: 81 percent / tetrahydrofuran / 18 h / 65 °C

3.1: 72 percent / KOH / methanol; H₂O / 18 h / 80 °C

With potassium hydroxide; sodium hydride; In tetrahydrofuran; methanol; dichloromethane; water; 1.1: Ene reaction / 2.1: Deprotonation / 2.2: Alkylation / 3.1: Hydrolysis;
DOI:10.1021/ol000044c