1-(2-cyclohexen-1-yl)-4-methyl-2-(2-oxo-2-phenylethyl)-1,2,4-triazolidine-3,5-dione

Base Information

Chemical Name:1-(2-cyclohexen-1-yl)-4-methyl-2-(2-oxo-2-phenylethyl)-1,2,4-triazolidine-3,5-dione
CAS No.:270063-67-7
Molecular Formula:C₁₇H₁₉N₃O₃
Molecular Weight:313.356
Hs Code.:

Synonyms:1-(2-cyclohexen-1-yl)-4-methyl-2-(2-oxo-2-phenylethyl)-1,2,4-triazolidine-3,5-dione

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Chemical Property of 1-(2-cyclohexen-1-yl)-4-methyl-2-(2-oxo-2-phenylethyl)-1,2,4-triazolidine-3,5-dione

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MSDS Files:: SDS file from LookChem

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Technology Process of 1-(2-cyclohexen-1-yl)-4-methyl-2-(2-oxo-2-phenylethyl)-1,2,4-triazolidine-3,5-dione

There total 2 articles about 1-(2-cyclohexen-1-yl)-4-methyl-2-(2-oxo-2-phenylethyl)-1,2,4-triazolidine-3,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 154228-83-8
1-(2-cyclohexen-1-yl)-4-methyl-1,2,4-triazolidine-3,5-dione

: 70-11-1
α-bromoacetophenone

: 270063-67-7
1-(2-cyclohexen-1-yl)-4-methyl-2-(2-oxo-2-phenylethyl)-1,2,4-triazolidine-3,5-dione

Guidance literature:: 1-(2-cyclohexen-1-yl)-4-methyl-1,2,4-triazolidine-3,5-dione; With sodium hydride; In tetrahydrofuran; at 65 ℃; for 3h;

α-bromoacetophenone; In tetrahydrofuran; at 65 ℃; for 18h; Further stages.;
DOI:10.1021/ol000044c

Reference yield:

: 110-83-8
cyclohexene

: 270063-67-7
1-(2-cyclohexen-1-yl)-4-methyl-2-(2-oxo-2-phenylethyl)-1,2,4-triazolidine-3,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: CH₂Cl₂ / 16 h / 20 °C

2.1: NaH / tetrahydrofuran / 3 h / 65 °C

2.2: 81 percent / tetrahydrofuran / 18 h / 65 °C

With sodium hydride; In tetrahydrofuran; dichloromethane; 1.1: Ene reaction / 2.1: Deprotonation / 2.2: Alkylation;
DOI:10.1021/ol000044c

Reference yield: 80.0%

: 77-78-1
dimethyl sulfate

: 270063-67-7
1-(2-cyclohexen-1-yl)-4-methyl-2-(2-oxo-2-phenylethyl)-1,2,4-triazolidine-3,5-dione

: 6-benzoyl-1-(2-cyclohexen-1-yl)-dihydro-3,5-dimethyl-1,3,5-triazine-2,4-(1H,3H)dione

Guidance literature:: 1-(2-cyclohexen-1-yl)-4-methyl-2-(2-oxo-2-phenylethyl)-1,2,4-triazolidine-3,5-dione; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

dimethyl sulfate; In tetrahydrofuran; at 20 ℃; for 12h; Further stages.;
DOI:10.1021/ol000044c