2-Butenoic acid, 3-(2-naphthalenyl)-, methyl ester, (2E)-

Base Information

Chemical Name:2-Butenoic acid, 3-(2-naphthalenyl)-, methyl ester, (2E)-
CAS No.:212078-20-1
Molecular Formula:C₁₅H₁₄O₂
Molecular Weight:226.275
Hs Code.:
Mol file:212078-20-1.mol

Synonyms:methyl (dimethoxyphophinothionyl)malonate;dimethyl (dimethoxyphosphinothioyl)malonate;Methyl (E)-(2-naphthyl)-3-methylacrylate;methyl (E)-3-(naphthalen-2-yl)-but-2-enoate;Propanedioic acid,(dimethoxyphosphinothioyl)-,dimethyl ester;methyl (E)-3-(2-naphthyl)crotonate;

Suppliers and Price of 2-Butenoic acid, 3-(2-naphthalenyl)-, methyl ester, (2E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(2E)-MethylEster3-(2-Naphthalenyl)-2-ButenoicAcid
10mg
$ 65.00

ChemScene
2-Butenoicacid,3-(2-naphthalenyl)-,methylester,(2E)-
1g
$ 825.00

Total 5 raw suppliers

Chemical Property of 2-Butenoic acid, 3-(2-naphthalenyl)-, methyl ester, (2E)-

Chemical Property:

Boiling Point:361.0±12.0 °C(Predicted)
PSA：26.30000
Density:1.107±0.06 g/cm3(Predicted)
LogP:3.41610

Purity/Quality:

≥95% ^*data from raw suppliers

(2E)-MethylEster3-(2-Naphthalenyl)-2-ButenoicAcid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Butenoic acid, 3-(2-naphthalenyl)-, methyl ester, (2E)-

There total 3 articles about 2-Butenoic acid, 3-(2-naphthalenyl)-, methyl ester, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 623-43-8
crotonic acid methyl ester

: 580-13-2
2-bromonaphthalene

: 51212-51-2
methyl (Z)-3-(naphthalen-2-yl)-but-2-enoate

: 212078-20-1
methyl (E)-3-(naphthalen-2-yl)-but-2-enoate

Guidance literature:: With N-Methyldicyclohexylamine; tetraethylammonium chloride; palladium diacetate; In N,N-dimethyl acetamide; at 95 - 100 ℃; for 16h;
DOI:10.1002/(SICI)1521-3765(19991105)5:11<3107::AID-CHEM3107>3.0.CO;2-#

Reference yield:

: 5927-18-4
trimethyl phosphonoacetate

: 93-08-3
methyl 2-naphthyl ketone

: 212078-20-1
methyl (E)-3-(naphthalen-2-yl)-but-2-enoate

Guidance literature:: trimethyl phosphonoacetate; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

methyl 2-naphthyl ketone; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo101849b