2,4,6-Tris(methoxymethoxy)benzaldehyde

Base Information

Chemical Name:2,4,6-Tris(methoxymethoxy)benzaldehyde
CAS No.:212265-19-5
Molecular Formula:C13H18O7
Molecular Weight:286.282
Hs Code.:
DSSTox Substance ID:DTXSID30440859
Nikkaji Number:J2.031.477J
Wikidata:Q82257305
Mol file:212265-19-5.mol

Synonyms:2,4,6-tris(methoxymethoxy)benzaldehyde;212265-19-5;Benzaldehyde, 2,4,6-tris(methoxymethoxy)-;DTXSID30440859;2,4,6-tris(methoxymethoxy)benzal-dehyde

Suppliers and Price of 2,4,6-Tris(methoxymethoxy)benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
2,4,6-Tris(methoxymethoxy)benzaldehyde
1g
$ 903.95

Total 2 raw suppliers

Chemical Property of 2,4,6-Tris(methoxymethoxy)benzaldehyde

Chemical Property:

PSA：72.45000
LogP:1.44720
XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:10
Exact Mass:286.10525291
Heavy Atom Count:20
Complexity:243

Purity/Quality:

99% ^*data from raw suppliers

2,4,6-Tris(methoxymethoxy)benzaldehyde ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COCOC1=CC(=C(C(=C1)OCOC)C=O)OCOC

Technology Process of 2,4,6-Tris(methoxymethoxy)benzaldehyde

There total 8 articles about 2,4,6-Tris(methoxymethoxy)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 850795-81-2
2,4,6-tris(methoxymethoxy)benzyl alcohol

: 212265-19-5
2,4,6-tris(O-methoxymethyl)benzaldehyde

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; for 1h;
DOI:10.1021/ja045520z

Reference yield: 87.0%

: 487-70-7
2,4,6-trihydroxybenzaldehyde

: 107-30-2
chloromethyl methyl ether

: 212265-19-5
2,4,6-tris(O-methoxymethyl)benzaldehyde

Guidance literature:: With potassium carbonate; In acetone; for 0.5h; Heating;
DOI:10.1080/00397919808004863

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 212265-19-5
2,4,6-tris(O-methoxymethyl)benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: POCl₃ / 0.33 h / 0 °C

1.2: acetonitrile / 18 h / 20 °C

2.1: 79.2 percent / H₂O / methanol / 4 h / 20 °C

3.1: 64.1 percent / DIPEA / CH₂Cl₂ / 0 °C

With water; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In methanol; dichloromethane; 1.1: Chlorination / 1.2: Substitution / 2.1: Hydrolysis / 3.1: Condensation;
DOI:10.1021/ja990591x