Silane, [[(1S,2S,4R,5R,6R)-6-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-4-(methoxy methoxy)-5-methyl-5-[(phenylmethoxy)methyl]bicyclo[2.2.1]hept-2-yl]oxy] (1,1-dimethylethyl)dimethyl-

Base Information

Chemical Name:Silane, [[(1S,2S,4R,5R,6R)-6-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-4-(methoxy methoxy)-5-methyl-5-[(phenylmethoxy)methyl]bicyclo[2.2.1]hept-2-yl]oxy] (1,1-dimethylethyl)dimethyl-
CAS No.:213816-63-8
Molecular Formula:C29H48O6Si
Molecular Weight:520.782
Hs Code.:

Silane,
[[(1S,2S,4R,5R,6R)-6-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-4-(methoxy
methoxy)-5-methyl-5-[(phenylmethoxy)methyl]bicyclo[2.2.1]hept-2-yl]oxy]
(1,1-dimethylethyl)dimethyl-

Synonyms:

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Chemical Property of Silane, [[(1S,2S,4R,5R,6R)-6-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-4-(methoxy methoxy)-5-methyl-5-[(phenylmethoxy)methyl]bicyclo[2.2.1]hept-2-yl]oxy] (1,1-dimethylethyl)dimethyl-

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Technology Process of Silane, [[(1S,2S,4R,5R,6R)-6-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-4-(methoxy methoxy)-5-methyl-5-[(phenylmethoxy)methyl]bicyclo[2.2.1]hept-2-yl]oxy] (1,1-dimethylethyl)dimethyl-

There total 8 articles about Silane, [[(1S,2S,4R,5R,6R)-6-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-4-(methoxy methoxy)-5-methyl-5-[(phenylmethoxy)methyl]bicyclo[2.2.1]hept-2-yl]oxy] (1,1-dimethylethyl)dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 100-39-0
benzyl bromide

: 213816-80-9
[(1R,2R,3R,4S,5S)-5-(tert-Butyl-dimethyl-silanyloxy)-3-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-methoxymethoxy-2-methyl-bicyclo[2.2.1]hept-2-yl]-methanol

: 213816-63-8
[(1S,2S,4R,5R,6R)-5-benzyloxymethyl-6-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-4-methoxymethoxy-5-methylbicyclo[2.2.1]hept-2-yloxy]-tert-butyldimethylsilane

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/S0040-4039(98)01385-9

Reference yield:

: 81997-76-4
(S,E)-3-(2,2-dimethyl-1,3-dioxolan-4-yl)-2-methylpropionic acid ethyl ester

: 213816-63-8
[(1S,2S,4R,5R,6R)-5-benzyloxymethyl-6-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-4-methoxymethoxy-5-methylbicyclo[2.2.1]hept-2-yloxy]-tert-butyldimethylsilane

Guidance literature:: Multi-step reaction with 5 steps

1: 69 percent / lithium diisopropylamide / tetrahydrofuran; hexane / 2 h / -78 °C

2: 100 percent / NaBH₄ / methanol / 0.25 h / 0 °C

3: 100 percent / imidazole / dimethylformamide / 10 h / 20 °C

4: 99 percent / LiAlH₄ / diethyl ether / 0.17 h / 0 °C

5: 94 percent / NaH / dimethylformamide / 12 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; lithium aluminium tetrahydride; sodium hydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(02)01474-6

Reference yield:

: 3-Methoxymethoxy-cyclopent-2-enone

: 213816-63-8
[(1S,2S,4R,5R,6R)-5-benzyloxymethyl-6-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-4-methoxymethoxy-5-methylbicyclo[2.2.1]hept-2-yloxy]-tert-butyldimethylsilane

Guidance literature:: Multi-step reaction with 5 steps

1: 69 percent / lithium diisopropylamide / tetrahydrofuran; hexane / 2 h / -78 °C

2: 100 percent / NaBH₄ / methanol / 0.25 h / 0 °C

3: 100 percent / imidazole / dimethylformamide / 10 h / 20 °C

4: 99 percent / LiAlH₄ / diethyl ether / 0.17 h / 0 °C

5: 94 percent / NaH / dimethylformamide / 12 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; lithium aluminium tetrahydride; sodium hydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(02)01474-6