3-nitro-9-isopropyl-9H-carbazole

Base Information

• Chemical Name: 3-nitro-9-isopropyl-9H-carbazole
• CAS No.: 22130-02-5
• Molecular Formula: C15H14N2O2
• Molecular Weight: 254.28400
• Mol file: 22130-02-5.mol

Synonyms:9-Isopropyl-3-nitro-9H-carbazole;3-nitro-9-isopropyl-9H-carbazole;3-Nitro-9-isopropyl-carbazole;9-isopropyl-3-nitrocarbazole;9-Isopropyl-3-nitro-carbazol;

Chemical Property of 3-nitro-9-isopropyl-9H-carbazole

Chemical Property:

• PSA: 50.75000
• LogP: 4.80680

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-nitro-9-isopropyl-9H-carbazole

There total 5 articles about 3-nitro-9-isopropyl-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

9-isopropyl-9H-carbazole (1484-09-9) → 3-nitro-9-isopropylcarbazole (22130-02-5)

Guidance literature:

With nitric acid; In acetic acid;

Reference yield: 79.0%

3-Nitro-carbazol (3077-85-8) + isopropyl bromide (75-26-3) → 3-nitro-9-isopropylcarbazole (22130-02-5)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 60 ℃; for 18h;

DOI:10.1021/jm011125x

Reference yield: 74.0%

9-isopropyl-9H-carbazole (1484-09-9) → 3-nitro-9-isopropylcarbazole (22130-02-5) + 1-nitro-9-isopropylcarbazole (111199-64-5)

Guidance literature:

With ammonium cerium(IV) nitrate; silica gel; In acetonitrile; at 70 - 75 ℃;

DOI:10.1080/00397919408012618

upstream raw materials:

9-isopropyl-9H-carbazole

3-Nitro-carbazol

isopropyl bromide

Downstream raw materials:

morpholine-4-carboxylic acid (9-isopropyl-4-methyl-9H-carbazol-3-yl)amide