9-Isopropyl-9H-carbazole

Base Information

• Chemical Name: 9-Isopropyl-9H-carbazole
• CAS No.: 1484-09-9
• Molecular Formula: C15H15 N
• Molecular Weight: 209.291
• Hs Code.: 2933990090
• European Community (EC) Number: 216-052-4
• UNII: C8E7ATK495
• DSSTox Substance ID: DTXSID2061723
• Nikkaji Number: J206.689K
• Wikidata: Q81989620
• Mol file: 1484-09-9.mol

Synonyms:9-Isopropyl-9H-carbazole;9-isopropylcarbazole;1484-09-9;9H-Carbazole, 9-(1-methylethyl)-;9-propan-2-ylcarbazole;Carbazole, 9-isopropyl-;N-Isopropylcarbazole;9-(propan-2-yl)-9H-carbazole;C8E7ATK495;9-(1-methylethyl)-9H-carbazole;EINECS 216-052-4;MFCD00046896;9-Isopropyl carbazole;Maybridge3_000552;UNII-C8E7ATK495;9-Isopropyl-9H-carbazole #;9H-Carbazole, 9-isopropyl-;SCHEMBL150044;DTXSID2061723;HMS1432J02;STK746423;AKOS001584885;CCG-103154;IDI1_011939;CS-0320907;FT-0633595;E85286;SR-01000389267;SR-01000389267-1

Chemical Property of 9-Isopropyl-9H-carbazole

Chemical Property:

• Vapor Pressure: 5.12E-05mmHg at 25°C
• Melting Point: 118-122oC
• Refractive Index: 1.5720 (estimate)
• Boiling Point: 348.2°Cat760mmHg
• Flash Point: 164.4°C
• PSA: 4.93000
• Density: 1.05g/cm³
• LogP: 4.37540
• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 209.120449483
• Heavy Atom Count: 16
• Complexity: 226

Purity/Quality:

97% ^*data from raw suppliers

9-ISOPROPYLCARBAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)N1C2=CC=CC=C2C3=CC=CC=C31

Technology Process of 9-Isopropyl-9H-carbazole

There total 9 articles about 9-Isopropyl-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

9H-carbazole (86-74-8,105184-46-1,97960-57-1) + isopropyl bromide (75-26-3) → 9-isopropyl-9H-carbazole (1484-09-9)

Guidance literature:

With tetrabutyl ammonium fluoride; potassium hydroxide; In acetone; for 3h; Heating;

DOI:10.1002/ejoc.201700602

Reference yield: 80.0%

N-isopropyl-[1-1'-biphenyl]-2-amine (1019616-33-1) → 9-isopropyl-9H-carbazole (1484-09-9)

Guidance literature:

With [bis(acetoxy)iodo]benzene; palladium diacetate; In toluene; at 20 ℃; for 4h;

DOI:10.1021/ja806543s

Reference yield: 69.0%

cis,trans-2,5-dimethoxytetrahydrofuran (696-59-3) + isopropylamine hydrochloride (15572-56-2) → 9-isopropyl-9H-carbazole (1484-09-9)

Guidance literature:

In water; benzene; Heating;

DOI:10.1016/S0040-4039(00)84467-6

upstream raw materials:

cis,trans-2,5-dimethoxytetrahydrofuran

isopropylamine hydrochloride

9H-carbazole

isopropyl bromide

Downstream raw materials:

3-nitro-9-isopropylcarbazole

1-nitro-9-isopropylcarbazole

9-isopropyl-3,6-diacetyl carbazole

3-bromo-N-isopropylcarbazole