Phosphinecarboxylic acid, ethoxyphenyl-, ethyl ester, oxide

Base Information

• Chemical Name: Phosphinecarboxylic acid, ethoxyphenyl-, ethyl ester, oxide
• CAS No.: 22779-69-7
• Molecular Formula: C₁₁H₁₅O₄P
• Molecular Weight: 242.211
• Mol file: 22779-69-7.mol

Synonyms:

Chemical Property of Phosphinecarboxylic acid, ethoxyphenyl-, ethyl ester, oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Phosphinecarboxylic acid, ethoxyphenyl-, ethyl ester, oxide

There total 1 articles about Phosphinecarboxylic acid, ethoxyphenyl-, ethyl ester, oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

diethyl phenylphosphonite (1638-86-4) + chloroformic acid ethyl ester (541-41-3) → Ethoxycarbonyl-phenylphosphinsaeure-ethylester (22779-69-7)

Guidance literature:

In tetrahydrofuran; for 1h; Product distribution; Heating; reaction with ClCONR₂ or BrCN or 2,4-dimethoxybromobenzene (NiCl₂);

DOI:10.1007/BF00810588

upstream raw materials:

diethyl phenylphosphonite

chloroformic acid ethyl ester