Quinoxaline, 1,2,3,4-tetrahydro-2-methyl-, (2R)-

Base Information

• Chemical Name: Quinoxaline, 1,2,3,4-tetrahydro-2-methyl-, (2R)-
• CAS No.: 24463-30-7
• Molecular Formula: C₉H₁₂N₂
• Molecular Weight: 148.208
• Mol file: 24463-30-7.mol

Synonyms:

Chemical Property of Quinoxaline, 1,2,3,4-tetrahydro-2-methyl-, (2R)-

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

(R)-2-Methyl-1,2,3,4-tetrahydroquinoxaline 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Quinoxaline, 1,2,3,4-tetrahydro-2-methyl-, (2R)-

There total 20 articles about Quinoxaline, 1,2,3,4-tetrahydro-2-methyl-, (2R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-methylquinoxaline (7251-61-8) → 2-methyl-1,2,3,4-tetrahydroquinoxaline (6640-55-7,24463-30-7,24463-31-8,49849-47-0)

Guidance literature:

With lithium borohydride; methyl iodide; In tetrahydrofuran; at 20 ℃; for 0.25h;

DOI:10.1002/jhet.5570420546

Reference yield: 95.0%

3-methyl-2-oxo-1,2-dihydroquinoxaline (14003-34-0) → 2-methyl-1,2,3,4-tetrahydroquinoxaline (6640-55-7,24463-30-7,24463-31-8,49849-47-0)

Guidance literature:

With tris(pentafluorophenyl)borate; In toluene; at 110 ℃; for 16h;

DOI:10.1039/c7gc03095a

Reference yield: 91.0%

pyruvic acid methyl ester (600-22-6) + 1,2-diamino-benzene (95-54-5) → 2-methyl-1,2,3,4-tetrahydroquinoxaline (6640-55-7,24463-30-7,24463-31-8,49849-47-0)

Guidance literature:

With tris(pentafluorophenyl)borate; In toluene; at 110 ℃; for 16h; Solvent; Temperature; Catalytic behavior;

DOI:10.1039/c7gc03095a

upstream raw materials:

2-methylquinoxaline

2-chloro-3-methylquinoxaline

1-(2-Aminophenyl)-4,5-dihydro-4-methyl-5-morpholino-1,2,3-triazole

3-methyl-2-oxo-1,2-dihydroquinoxaline

Downstream raw materials:

2-<(E)-2-Phenylethenyl>chinoxalin

2-phenethylquinoxaline

2-methylquinoxaline

1-nitroso-2,4-dimetil-1,2,3,4-tetraidrochinossalina