Bis(trifluoroacetic acid)ethylene ester

Base Information

• Chemical Name: Bis(trifluoroacetic acid)ethylene ester
• CAS No.: 2613-44-7
• Molecular Formula: C6H4F6O4
• Molecular Weight: 254.086
• Hs Code.: 2915900090
• Mol file: 2613-44-7.mol

Synonyms:1,2-Bis-trifluoracetoxy-aethan;1,2-bis-trifluoroacetoxy-ethane;Acetic acid, trifluoro-, 1,2-ethanediyl ester;trifluoro-acetic acid,1,2-ethanediyl ester;

Chemical Property of Bis(trifluoroacetic acid)ethylene ester

Chemical Property:

• PSA: 52.60000
• LogP: 1.19740

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bis(trifluoroacetic acid)ethylene ester

There total 11 articles about Bis(trifluoroacetic acid)ethylene ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

ethane (74-84-0) + trifluoroacetic acid (76-05-1) → chloroethane (75-00-3) + ethyl trifluoroacetate, (383-63-1) + 1,2-bis(trifluoroacetyl)ethane (2613-44-7)

Guidance literature:

With ammonium iodate; potassium chloride; at 180 ℃; for 1h; under 15526.6 Torr; Sealed tube;

DOI:10.1021/ja502657g

Reference yield:

ethane (74-84-0) + trifluoroacetic acid (76-05-1) + trifluoroacetic anhydride (407-25-0) → ethyl trifluoroacetate, (383-63-1) + 1,2-bis(trifluoroacetyl)ethane (2613-44-7)

Guidance literature:

With iodic acid; at 150 ℃; for 3h; under 25858.1 Torr; Reagent/catalyst; Temperature;

Reference yield:

ethane (74-84-0) + iodine tris(trifluoroacetate) (14353-86-7) + trifluoroacetic acid (76-05-1) → ethyl trifluoroacetate, (383-63-1) + 1,2-bis(trifluoroacetyl)ethane (2613-44-7)

Guidance literature:

With trifluoroacetic anhydride; at 150 ℃; for 3h; under 25858.1 Torr;

upstream raw materials:

ethane

trifluoroacetic acid

trifluoroacetyl peroxide

propionyltrifluoroacetyl peroxide

Downstream raw materials:

1,2-bis-(1,1,2,2-tetrafluoro-ethoxy)-ethane

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