Ethanone, 1-[3,4,6-trimethoxy-2-(2-propenyl)phenyl]-

Base Information

Chemical Name:Ethanone, 1-[3,4,6-trimethoxy-2-(2-propenyl)phenyl]-
CAS No.:263138-69-8
Molecular Formula:C14H18O4
Molecular Weight:250.295
Hs Code.:

Synonyms:

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Chemical Property of Ethanone, 1-[3,4,6-trimethoxy-2-(2-propenyl)phenyl]-

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Technology Process of Ethanone, 1-[3,4,6-trimethoxy-2-(2-propenyl)phenyl]-

There total 14 articles about Ethanone, 1-[3,4,6-trimethoxy-2-(2-propenyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 100612-88-2
1-(5-(allyloxy)-2,4-dimethoxyphenyl)ethanone

: 77-78-1
dimethyl sulfate

: 263138-69-8
2-allyl-3,4,6-trimethoxyacetophenone

Guidance literature:: 1-(5-(allyloxy)-2,4-dimethoxyphenyl)ethanone; at 170 ℃;

dimethyl sulfate; With potassium carbonate; In acetone;
DOI:10.1016/S0040-4020(01)00963-2

Reference yield:

: 100612-88-2
1-(5-(allyloxy)-2,4-dimethoxyphenyl)ethanone

: 263138-69-8
2-allyl-3,4,6-trimethoxyacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 2 h / 160 °C

2: 2.03 g / K₂CO₃ / acetone / 20 h / Heating

With potassium carbonate; In acetone; 1: Claisen rearrangement / 2: Methylation;

Reference yield:

: 22280-95-1
4-allyloxy-3-methoxybenzaldehyde

: 263138-69-8
2-allyl-3,4,6-trimethoxyacetophenone

Guidance literature:: Multi-step reaction with 6 steps

1: magnesium monoperoxyperphthalic acid hexahydrate / methanol / 48 h / 25 °C

2: 11.20 g / silica gel; conc.HCl / CH₂Cl₂ / 12 h

3: 91 percent / K₂CO₃ / acetone / 18 h / Heating

4: 67 percent / trifluoroacetic acid anhydride / CH₂Cl₂ / 60 h / 25 °C

5: 2 h / 160 °C

6: 2.03 g / K₂CO₃ / acetone / 20 h / Heating

With hydrogenchloride; magnesium monoperoxyperphthalic acid hexahydrate; silica gel; potassium carbonate; trifluoroacetic anhydride; In methanol; dichloromethane; acetone; 1: Oxidation / 2: Hydrolysis / 3: Methylation / 4: Acylation / 5: Claisen rearrangement / 6: Methylation;