Pentanamide, N-(4-bromophenyl)-5-chloro-

Base Information

Chemical Name:Pentanamide, N-(4-bromophenyl)-5-chloro-
CAS No.:27471-42-7
Molecular Formula:C11H13BrClNO
Molecular Weight:290.587
Hs Code.:
DSSTox Substance ID:DTXSID701285761

Synonyms:Pentanamide, N-(4-bromophenyl)-5-chloro-;N-(4-bromophenyl)-5-chloropentanamide;27471-42-7;SCHEMBL4420939;DTXSID701285761

Suppliers and Price of Pentanamide, N-(4-bromophenyl)-5-chloro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Pentanamide, N-(4-bromophenyl)-5-chloro-

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:288.98690
Heavy Atom Count:15
Complexity:193

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1NC(=O)CCCCCl)Br

Technology Process of Pentanamide, N-(4-bromophenyl)-5-chloro-

There total 1 articles about Pentanamide, N-(4-bromophenyl)-5-chloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1119-46-6
5-chloro-valeric acid

: 106-40-1
4-bromo-aniline

: 27471-42-7
N-(4-Bromophenyl)-5-chloropentanamide

Guidance literature:: With hydrogenchloride; thionyl chloride; triethylamine; In dichloromethane; toluene;

Reference yield:

: 27471-42-7
N-(4-Bromophenyl)-5-chloropentanamide

: 1-benzyl-7-bromo-1,2,3,4-tetrahydro-benzo[b][1,8]naphthyridine

Guidance literature:: Multi-step reaction with 2 steps

1: POCl₃ / 6 h / 75 °C

2: 2.4 g / dimethylformamide / 15 h / 160 °C

With trichlorophosphate; In N,N-dimethyl-formamide; 1: Vilsmeier-Haack reaction;
DOI:10.1021/jm049499o

Reference yield:

: 27471-42-7
N-(4-Bromophenyl)-5-chloropentanamide

: 1-(3,4-dihydro-2H-1-oxa-9-aza-anthracen-6-yl)-3-phenyl-propan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: POCl₃ / 6 h / 75 °C

2.1: 28 percent / aq. HCl / 10 h / Heating

3.1: n-BuLi / hexane; tetrahydrofuran / -70 - -20 °C

3.2: 38 percent / tetrahydrofuran; hexane / -70 °C

With hydrogenchloride; n-butyllithium; trichlorophosphate; In tetrahydrofuran; hexane; 1.1: Vilsmeier-Haack reaction;
DOI:10.1021/jm049499o