Cyclohexanol, 1-(tributylstannyl)-

Base Information

Chemical Name:Cyclohexanol, 1-(tributylstannyl)-
CAS No.:27490-36-4
Molecular Formula:C18H38OSn
Molecular Weight:389.209
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexanol, 1-(tributylstannyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Cyclohexanol, 1-(tributylstannyl)-

There total 1 articles about Cyclohexanol, 1-(tributylstannyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 27262-82-4
tributylstannylmagnesium chloride

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 27490-36-4
(CH₃(CH₂)3)3SnC₆H₁₀(OH)

Guidance literature:: In diethyl ether;

Reference yield: 78.0%

: 27490-36-4
(CH₃(CH₂)3)3SnC₆H₁₀(OH)

: 103-71-9
phenyl isocyanate

: 136052-31-8
(C₄H₉)3SnC₆H₁₀OCONHC₆H₅

Guidance literature:: In pentane; byproducts: 1,3-diphenylurea; react. under an inert atmosphere; addn. of phenyl isocyanate soln. to Sn-compound in soln. at room temp. (molar ratio 2:1), stirred at reflux for 5h, pptn.; ppt. removed by filtration, cooled to -20°C overnight, pptn. of last traces of diphenylurea, solvent and unreacted isocyanate removed under reduced pressure;

Reference yield: 73.0%

: 79-37-8
oxalyl dichloride

: 27490-36-4
(CH₃(CH₂)3)3SnC₆H₁₀(OH)

: 136052-40-9
tributylstannylcyclohexyl oxalate

Guidance literature:: With pyridine; In diethyl ether; byproducts: C5H5NHCl; addn. of oxalyl chloride in ether to stannylalcohol and pyridine in ether, mixt. stirred for 5h at room temp. (molar ratio Sn-alcohol:oxalyl chloride (2:1); ppt. of pyridine hydrochloride filtered off, react. mixt. washed with water;