N-Methyl-N-nitrosobenzamide

Base Information

Chemical Name:N-Methyl-N-nitrosobenzamide
CAS No.:63412-06-6
Molecular Formula:C8H8N2O2
Molecular Weight:164.164
Hs Code.:2924299090
DSSTox Substance ID:DTXSID6020850
Nikkaji Number:J3.524F
Wikidata:Q81983628
Mol file:63412-06-6.mol

Synonyms:N-methyl-N-nitrosobenzamide

Suppliers and Price of N-Methyl-N-nitrosobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 10 raw suppliers

Chemical Property of N-Methyl-N-nitrosobenzamide

Chemical Property:

Vapor Pressure:0.0361mmHg at 25°C
Refractive Index:1.6000 (estimate)
Boiling Point:241.3°Cat760mmHg
PKA:-2.60±0.70(Predicted)
Flash Point:99.7°C
PSA：49.74000
Density:1.15g/cm³
LogP:1.44000
Storage Temp.:-20°C
XLogP3:0.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:164.058577502
Heavy Atom Count:12
Complexity:176

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C(=O)C1=CC=CC=C1)N=O

Technology Process of N-Methyl-N-nitrosobenzamide

There total 5 articles about N-Methyl-N-nitrosobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 88070-48-8
N-methylbenzamide

: 63412-06-6
N-methyl-N-nitrosobenzamide

Guidance literature:: With sodium acetate; Nitrogen dioxide; In dichloromethane; at -20 ℃;
DOI:10.1021/jo00192a014

Reference yield: 46.0%

: 88070-48-8
N-methylbenzamide

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 63412-06-6
N-methyl-N-nitrosobenzamide

Guidance literature:: With n-Butyl nitrite; In 1,2-dichloro-ethane; at 40 ℃; for 3h;
DOI:10.1021/acs.joc.7b00570

Reference yield:

: 98-88-4
benzoyl chloride

: 63412-06-6
N-methyl-N-nitrosobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane; water / 1 h / 0 - 20 °C / Inert atmosphere

2: tert.-butylnitrite / dichloromethane / 1 h / 20 °C / Inert atmosphere

With tert.-butylnitrite; triethylamine; In dichloromethane; water;
DOI:10.1021/acs.joc.9b01699