N-Ethylbenzamide

Base Information

• Chemical Name: N-Ethylbenzamide
• CAS No.: 614-17-5
• Molecular Formula: C9H11 N O
• Molecular Weight: 149.192
• Hs Code.: 2924299090
• European Community (EC) Number: 664-988-0
• NSC Number: 20558
• UNII: SW509B0V2A
• DSSTox Substance ID: DTXSID10210315
• Nikkaji Number: J54.488D
• Wikidata: Q72472771
• ChEMBL ID: CHEMBL500597
• Mol file: 614-17-5.mol

Synonyms:N-ethylbenzamide

Chemical Property of N-Ethylbenzamide

Chemical Property:

• Vapor Pressure: 0.000395mmHg at 25°C
• Melting Point: 70.5°C
• Refractive Index: 1.5279 (estimate)
• Boiling Point: 317℃
• Flash Point: 184℃
• PSA: 29.10000
• Density: 1.019
• LogP: 1.82720
• XLogP3: 1.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 149.084063974
• Heavy Atom Count: 11
• Complexity: 128

Purity/Quality:

99% ^*data from raw suppliers

N-ETHYLBENZAMIDE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCNC(=O)C1=CC=CC=C1

Technology Process of N-Ethylbenzamide

There total 136 articles about N-Ethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

trimethyl((2-phenylbut-2-yl)peroxy)silane + benzamide (55-21-0,27208-38-4) → N-ethylbenzamide (614-17-5)

Guidance literature:

With copper(l) iodide; 1,10-Phenanthroline; In benzene; at 60 ℃; for 2h; Inert atmosphere;

DOI:10.1002/chem.201702217

Reference yield: 99.0%

ethanamine hydrochloride (557-66-4) + benzaldehyde (100-52-7) → N-ethylbenzamide (614-17-5)

Guidance literature:

With tert.-butylhydroperoxide; copper(l) iodide; sodium hydrogencarbonate; In decane; at 80 ℃; Further Variations:; Catalysts; Reagents; Solvents; Product distribution;

DOI:10.1021/ja064315b

Reference yield: 99.0%

trimethyl((3-phenylpentan-3-yl)peroxy)silane + benzamide (55-21-0,27208-38-4) → N-ethylbenzamide (614-17-5)

Guidance literature:

With copper(l) iodide; 1,10-Phenanthroline; In benzene; at 60 ℃; for 2h; Temperature; Time; Catalytic behavior; Inert atmosphere;

DOI:10.1002/chem.201702217

upstream raw materials:

ethanol

ethylthiocarbamic acid benzoic acid-thioanhydride

ethyl carbamoyl chloride

ethyl-carbamoyl azide

Downstream raw materials:

N-ethyl-N-(4-nitro-benzenesulfenyl)-benzamide

1-ethyl-5-diphenyl-1H-1,2,3,4-tetrazole

N-ethyl-N-chloro-benzamide

N-ethylchloro(phenyl)methanimine