N-(4-cyanophenyl)propanamide

Base Information

• Chemical Name: N-(4-cyanophenyl)propanamide
• CAS No.: 314764-76-6
• Molecular Formula: C10H10N2O
• Molecular Weight: 174.202
• Mol file: 314764-76-6.mol

Synonyms:N-(4-cyanophenyl)propanamide;4-Propionylamino-benzonitril;N-(4-Cyano-phenyl)-propionamide;4-propionylamino-benzonitrile;

Chemical Property of N-(4-cyanophenyl)propanamide

Chemical Property:

• Melting Point: 169 °C (H2O)
• PSA: 52.89000
• LogP: 1.97978

Purity/Quality:

99% ^*data from raw suppliers

N-(4-cyanophenyl)propanamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(4-cyanophenyl)propanamide

There total 5 articles about N-(4-cyanophenyl)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

propionic acid (802294-64-0,79-09-4) + 4-Aminobenzonitrile (873-74-5) → N-(4-cyanophenyl)propionamide (314764-76-6)

Guidance literature:

With fluorosulfonyl fluoride; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 5h;

DOI:10.1039/c9ob00699k

Reference yield: 38.0%

propionyl chloride (79-03-8) + 4-Aminobenzonitrile (873-74-5) → N-(4-cyanophenyl)propionamide (314764-76-6)

Guidance literature:

In dichloromethane; at 20 ℃; Schlenk technique;

DOI:10.1039/c4dt00372a

Reference yield:

4-nitro-aniline (100-01-6,104810-17-5) → N-(4-cyanophenyl)propionamide (314764-76-6)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrochloric acid / Diazotization_.Behandeln der Diazoniumchloridloesung mit Kaliumkupfercyanuer

2: tin dichloride; hydrochloric acid

With hydrogenchloride; tin(ll) chloride;

upstream raw materials:

propionic acid anhydride

4-Aminobenzonitrile

4-nitro-aniline

4-nitrobenzonitrile

Downstream raw materials:

(Z)-N-(4-(5-(4-methoxybenzylidene)-4-oxo-4,5-dihydrothiazol-2-yl)phenyl)propionamide

C₁₀H₉ClN₂

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