1-(3-Methyl-2,3-dihydro-1H-indol-1-yl)ethan-1-one

Base Information

Chemical Name:1-(3-Methyl-2,3-dihydro-1H-indol-1-yl)ethan-1-one
CAS No.:31676-46-7
Molecular Formula:C11H13NO
Molecular Weight:175.23
Hs Code.:
DSSTox Substance ID:DTXSID90553454
Nikkaji Number:J1.914.876I
Mol file:31676-46-7.mol

Synonyms:31676-46-7;1-(3-Methyl-2,3-dihydro-1H-indol-1-yl)ethan-1-one;1-(3-METHYL-2,3-DIHYDROINDOL-1-YL)ETHANONE;SCHEMBL14294095;DTXSID90553454

Suppliers and Price of 1-(3-Methyl-2,3-dihydro-1H-indol-1-yl)ethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-(3-Methyl-2,3-dihydro-1H-indol-1-yl)ethan-1-one

Chemical Property:

PSA：20.31000
LogP:2.22160
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:175.099714038
Heavy Atom Count:13
Complexity:214

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CN(C2=CC=CC=C12)C(=O)C

Technology Process of 1-(3-Methyl-2,3-dihydro-1H-indol-1-yl)ethan-1-one

There total 1 articles about 1-(3-Methyl-2,3-dihydro-1H-indol-1-yl)ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 115802-63-6
N-(2-bromophenyl)-N-methyl-p-toluenesulfonamide

: 31676-46-7
1-(3-methylindolin-1-yl)ethanone

: 4375-15-9
3-methyl-2,3-dihydro-1H-indole

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; tert-butyl alcohol; In tetrahydrofuran; for 0.166667h; Ambient temperature;
DOI:10.1016/S0040-4039(00)74317-6

Reference yield: 97.0%

: 31676-46-7
1-(3-methylindolin-1-yl)ethanone

: 70-55-3
toluene-4-sulfonamide

: 1612872-76-0
N-(1-acetyl-3-methylindolin-7-yl)-4-methylbenzenesulfonamide

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; [bis(acetoxy)iodo]benzene; silver(I) acetate; silver trifluoromethanesulfonate; acetic acid; In 1,2-dichloro-ethane; at 100 ℃; for 16h; Inert atmosphere; Sealed tube; Schlenk technique;
DOI:10.1016/j.tetlet.2019.03.069

Reference yield: 92.0%

: 941-55-9
4-toluenesulfonyl azide

: 31676-46-7
1-(3-methylindolin-1-yl)ethanone

: 1612872-76-0
N-(1-acetyl-3-methylindolin-7-yl)-4-methylbenzenesulfonamide

Guidance literature:: With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; sodium acetate; silver(I) triflimide; In 1,2-dichloro-ethane; at 25 ℃; for 6h; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo5018475