N,N-bis(4-dimethylaminophenyl)nitrous amide

Base Information

• Chemical Name: N,N-bis(4-dimethylaminophenyl)nitrous amide
• CAS No.: 13916-80-8
• Molecular Formula: C₁₆H₂₀N₄O
• Molecular Weight: 284.361
• Hs Code.: 2928000090
• NSC Number: 56922
• DSSTox Substance ID: DTXSID00930378
• Wikidata: Q82905713
• Mol file: 13916-80-8.mol

Synonyms:13916-80-8;N,N-bis(4-dimethylaminophenyl)nitrous amide;N,N-bis[4-(dimethylamino)phenyl]nitrous amide;NSC56922;SCHEMBL11419536;DTXSID00930378;NSC-56922;1,4-Benzenediamine,N1-[4-(dimethylamino)phenyl]-N4,N4-dimethyl-N1-nitroso-;CID 245212

Chemical Property of N,N-bis(4-dimethylaminophenyl)nitrous amide

Chemical Property:

• Vapor Pressure: 3.85E-09mmHg at 25°C
• Melting Point: 239-240 °C
• Boiling Point: 473.7°Cat760mmHg
• PKA: 4.34±0.12(Predicted)
• Flash Point: 240.3°C
• PSA: 39.15000
• Density: 1.07g/cm³
• LogP: 3.63810
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 4
• Exact Mass: 284.16371127
• Heavy Atom Count: 21
• Complexity: 290

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=CC=C(C=C1)N(C2=CC=C(C=C2)N(C)C)N=O

Technology Process of N,N-bis(4-dimethylaminophenyl)nitrous amide

There total 4 articles about N,N-bis(4-dimethylaminophenyl)nitrous amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4'-bis(dimethylamino)diphenylamine (637-31-0) → Bis-<4-dimethylamino-phenyl>-nitrosamin (13916-80-8)

Guidance literature:

With acetic acid; sodium nitrite;

Reference yield:

tetrakis-(4-dimethylamino-phenyl)-hydrazine (1990-18-7) → Bis-<4-dimethylamino-phenyl>-nitrosamin (13916-80-8)

Guidance literature:

With diethyl ether; nitrogen oxides;

Reference yield:

4,4'-bis(dimethylamino)diphenylamine (637-31-0) + acetic acid (64-19-7,77671-22-8) → Bis-<4-dimethylamino-phenyl>-nitrosamin (13916-80-8)

Guidance literature:

DOI:10.1155/EDR.2001.29

upstream raw materials:

4,4'-bis(dimethylamino)diphenylamine

tetrakis-(4-dimethylamino-phenyl)-hydrazine

diethyl ether

acetic acid

Downstream raw materials:

4,4'-bis(dimethylamino)diphenylamine

ammonia

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