1-CHLORO-2-IODO-3-NITRO-BENZENE

Base Information

• Chemical Name: 1-CHLORO-2-IODO-3-NITRO-BENZENE
• CAS No.: 32337-97-6
• Molecular Formula: C6H3ClINO2
• Molecular Weight: 283.453

Synonyms:3-Chloro-2-iodonitrobenzol;Benzene,1-chloro-2-iodo-3-nitro;3-chloro-2-iodo-1-nitrobenzene;1-chloro-2-iodo-3-nitro-benzene;1-Chlor-2-jod-3-nitro-benzol;

Chemical Property of 1-CHLORO-2-IODO-3-NITRO-BENZENE

Chemical Property:

• Melting Point: 100-101 °C
• Boiling Point: 305.0±27.0 °C(Predicted)
• PSA: 45.82000
• Density: 2.094±0.06 g/cm3(Predicted)
• LogP: 3.37600
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

1-Chloro-2-iodo-3-nitrobenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-CHLORO-2-IODO-3-NITRO-BENZENE

There total 6 articles about 1-CHLORO-2-IODO-3-NITRO-BENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2-chloro-6-nitroaniline (769-11-9) → 1-chloro-2-iodo-3-nitrobenzene (32337-97-6)

Guidance literature:

2-chloro-6-nitroaniline; With hydrogenchloride; sodium nitrite; at 0 ℃; for 0.25h;

With potassium iodide; at 20 ℃;

DOI:10.1021/jm0300835

Reference yield:

2-iodochlorobenzene (615-41-8) + nitric acid (7697-37-2,78989-43-2) → 2-chloro-1-iodo-3-nitro-benzene (683238-59-7) + 1-chloro-2-iodo-3-nitrobenzene (32337-97-6) + 1-chloro-2-iodo-4-nitrobenzene (74534-15-9) + 3-chloro-4-iodonitrobenzene (41252-96-4)

Guidance literature:

Reference yield:

3-Nitrochlorobenzene (121-73-3) → 1-chloro-2-iodo-3-nitrobenzene (32337-97-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 46 percent / methoxyamine hydrochloride; cuprous chloride; potassium tert-butoxide / dimethylformamide / 1 h

2.1: aq. HCl; NaNO₂ / 0.25 h / 0 °C

2.2: 75 percent / aq. KI / 20 °C

With hydrogenchloride; potassium tert-butylate; N-methoxylamine hydrochloride; copper(l) chloride; sodium nitrite; In N,N-dimethyl-formamide;

DOI:10.1021/jm0300835

upstream raw materials:

2-chloro-6-nitroaniline

2-iodochlorobenzene

nitric acid

3-Nitrochlorobenzene

Downstream raw materials:

3-iodo-4-chloroaniline

1-chloro-2-(3-methylbut-2-enyl)-3-nitrobenzene

3-chloro-2-iodobenzenamine

2-oxo-1,2,3,4-tetrahydroquinoline-5-carbonitrile

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