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Plumbane, ethyltriphenyl-

Base Information
  • Chemical Name:Plumbane, ethyltriphenyl-
  • CAS No.:33733-94-7
  • Molecular Formula:C20H20Pb
  • Molecular Weight:467.579
  • Hs Code.:
Plumbane, ethyltriphenyl-

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Chemical Property of Plumbane, ethyltriphenyl-
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Technology Process of Plumbane, ethyltriphenyl-

There total 5 articles about Plumbane, ethyltriphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With methanol; water; methyl iodide; In tetrahydrofuran; addn. of MeI to Ph3PbCH2Li in THF (N2, -50°C), stirred (30 min),addn. of MeOH, addn. of water; extn. with CHCl3, org. layers washed with water, dried (Na2SO4), evapn., chromy. (Al2O3, benzine), recrystn. (MeOH);
Guidance literature:
With water; methyl iodide; In tetrahydrofuran; addn. of MeI to Ph3PbCH2Li in THF (N2, -50°C), stirred (1 h, room temp.), addn. of water; extn. with CHCl3, org. layers washed with water, dried (Na2SO4), evapn., chromy. (Al2O3, benzine), fractionated crystn. (MeOH);
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