9H-Xanthen-9-amine

Base Information

• Chemical Name: 9H-Xanthen-9-amine
• CAS No.: 35598-63-1
• Molecular Formula: C13H11NO
• Molecular Weight: 197.236
• Hs Code.: 2932999099
• Mol file: 35598-63-1.mol

Synonyms:xanthen-9-ylamine;Xanthen-9-ylamin;9H-xanthen-9-ylamine;9-Xanthenylamin;9-Amino-xanthen;10-aminoxanthene;

Chemical Property of 9H-Xanthen-9-amine

Chemical Property:

• Melting Point: 59-61 °C
• Boiling Point: 305.6±41.0 °C(Predicted)
• PKA: 8.22±0.20(Predicted)
• PSA: 35.25000
• Density: 1?+-.0.06 g/cm3(Predicted)
• LogP: 3.54070
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

99%min ^*data from raw suppliers

9h-Xanthen-9-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9H-Xanthen-9-amine

There total 2 articles about 9H-Xanthen-9-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzylxanthone imine (6229-07-8) + chlorobenzene (108-90-7) → benzophenone (119-61-9) + xanth-9-one (90-47-1) + 9H-xanthen-9-ylamine (35598-63-1) + Benzhydrylamine (91-00-9)

Guidance literature:

N-benzylxanthone imine; chlorobenzene; With cesium hydroxide monohydrate; bis(η3-allyl-μ-chloropalladium(II)); tricyclohexylphosphine; In toluene; for 24h; Inert atmosphere; Reflux;

With hydrogenchloride; water; Inert atmosphere;

DOI:10.1021/ol802070d

Reference yield:

9H-xanthene-9-thione (492-21-7) → 9H-xanthen-9-ylamine (35598-63-1)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; hydroxylamine hydrochloride

2: ethanol; sodium

With pyridine; ethanol; hydroxylamine hydrochloride; sodium;

DOI:10.1039/jr9510000757

Reference yield: 84.0%

9H-xanthen-9-ylamine (35598-63-1) + C31H28Cl3N3NiO5 → C44H37Cl3N4NiO5

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In acetonitrile; at 20 ℃;

DOI:10.1007/s00726-018-2677-5

upstream raw materials:

9H-xanthene-9-thione

N-benzylxanthone imine

chlorobenzene

Downstream raw materials:

N-(9H-xanthen-9-yl)acetamide

N-(9-Xanthenyl)harnstoff

9-hydroxyxanthene

dixanthyl ether

Refernces