Hydrazinecarboxylic acid, [2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethylidene]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Hydrazinecarboxylic acid, [2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethylidene]-, 1,1-dimethylethyl ester
CAS No.:357401-17-3
Molecular Formula:C22H28N2O4
Molecular Weight:384.475
Hs Code.:
Mol file:357401-17-3.mol

Synonyms:N'-(2-Benzyloxy-1-benzyloxymethyl-ethylidene)-hydrazinecarboxylic acid tert-butyl ester;

Suppliers and Price of Hydrazinecarboxylic acid, [2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethylidene]-, 1,1-dimethylethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Hydrazinecarboxylic acid, [2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethylidene]-, 1,1-dimethylethyl ester

Chemical Property:

PSA：69.15000
LogP:4.69160

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Hydrazinecarboxylic acid, [2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethylidene]-, 1,1-dimethylethyl ester

There total 2 articles about Hydrazinecarboxylic acid, [2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethylidene]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6972-79-8
dibenzyl glycerol

: 357401-17-3
1,3-dibenzyloxyacetone t-butyloxycarbonyl-hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOCl; TEMPO; NaHCO₃ / acetonitrile / 1 h / 0 - 5 °C

2: 6.05 kg / heptane; toluene / 1 h / 70 °C

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium hydrogencarbonate; In n-heptane; toluene; acetonitrile;
DOI:10.1016/S0040-4020(01)00895-X