Benzenamine, 4-methyl-N-[3-(4-methylphenyl)-4-phenyl-2(3H)-thiazolylidene]-

Base Information

• Chemical Name: Benzenamine, 4-methyl-N-[3-(4-methylphenyl)-4-phenyl-2(3H)-thiazolylidene]-
• CAS No.: 36220-33-4
• Molecular Formula: C₂₃H₂₀N₂S
• Molecular Weight: 356.491
• DSSTox Substance ID: DTXSID001149388

Synonyms:36220-33-4;Benzenamine, 4-methyl-N-[3-(4-methylphenyl)-4-phenyl-2(3H)-thiazolylidene]-;Oprea1_753103;DTXSID001149388;AKOS000987567;NCGC00328176-01;AB01104157-03;Z56754053;4-Methyl-N-[3-(4-methylphenyl)-4-phenyl-2(3H)-thiazolylidene]benzenamine;4-methyl-N-[(2Z)-3-(4-methylphenyl)-4-phenyl-1,3-thiazol-2(3H)-ylidene]aniline

Chemical Property of Benzenamine, 4-methyl-N-[3-(4-methylphenyl)-4-phenyl-2(3H)-thiazolylidene]-

Chemical Property:

• XLogP3: 6.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 356.13471982
• Heavy Atom Count: 26
• Complexity: 518

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)N=C2N(C(=CS2)C3=CC=CC=C3)C4=CC=C(C=C4)C

Technology Process of Benzenamine, 4-methyl-N-[3-(4-methylphenyl)-4-phenyl-2(3H)-thiazolylidene]-

There total 3 articles about Benzenamine, 4-methyl-N-[3-(4-methylphenyl)-4-phenyl-2(3H)-thiazolylidene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetophenone (98-86-2) + N,N'-Bis(p-tolyl)thiourea (621-01-2) → (4-phenyl-3-p-tolyl-3H-thiazol-2-ylidene)-p-tolyl-amine (36220-33-4)

Guidance literature:

Multistep reaction; (i) Br₂, EtOH, (ii) /BRN= 986456/;

Reference yield:

N,N-di-p-tolyl-thiourea (73901-66-3) + α-bromoacetophenone (70-11-1) → (4-phenyl-3-p-tolyl-3H-thiazol-2-ylidene)-p-tolyl-amine (36220-33-4)

Guidance literature:

With ethanol;

Reference yield:

→ (4-phenyl-3-p-tolyl-3H-thiazol-2-ylidene)-p-tolyl-amine (36220-33-4)

Guidance literature:

4-Methylphenylamin VIb,p-Toluidin;

DOI:10.1248/cpb.26.3017

upstream raw materials:

N,N-di-p-tolyl-thiourea

α-bromoacetophenone

acetophenone

N,N'-Bis(p-tolyl)thiourea

Downstream raw materials:

3-p-tolyl-4-phenyl-2-oxa-4-thiazoline

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