1,2-Azaborine, 1,2-dihydro-1-methyl-2-phenyl-

Base Information

Chemical Name:1,2-Azaborine, 1,2-dihydro-1-methyl-2-phenyl-
CAS No.:386708-26-5
Molecular Formula:C11H12BN
Molecular Weight:169.034
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Azaborine, 1,2-dihydro-1-methyl-2-phenyl-

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Technology Process of 1,2-Azaborine, 1,2-dihydro-1-methyl-2-phenyl-

There total 7 articles about 1,2-Azaborine, 1,2-dihydro-1-methyl-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 2,3-dihydro-1-methyl-2-phenyl-1H-1,2-azaborol-3-yllithium

: 75-09-2
dichloromethane

: 386708-26-5
1,2-dihydro-1-methyl-2-phenyl-1,2-azaborine

Guidance literature:: With lithium diisopropyl amide; In diethyl ether; dichloromethane; under N2; a soln. of lithium diisopropylamide in (CH3CH2)2O was added toa suspn. of 2,3-dihydro-1-methyl-2-phenyl-1H-1,2-azaborol-3-yllithium i n CH2Cl2 at -78°C, the mixt. was stirred at -78°C for 2 h,warmed to 25°C for 4 h; the volatiles were removed in vac., the residue was extd. with pentane and filtered, pentane was removed, the residue was chromd. (SiO2, pentane); elem. anal.;
DOI:10.1021/om0106635

Reference yield:

: 2,3-dihydro-1-trimethylsilyl-2-phenyl-1H-1,2-azaborol-3-yllithium

: 386708-26-5
1,2-dihydro-1-methyl-2-phenyl-1,2-azaborine

Guidance literature:: Multi-step reaction with 4 steps

1: dichloromethane; diethyl ether

2: Bu₄NF / tetrahydrofuran

3: toluene

4: dimethylsulfoxide-d6

With Bu₄NF; In tetrahydrofuran; dimethylsulfoxide-d6; diethyl ether; dichloromethane; toluene;
DOI:10.1021/om049399g

Reference yield:

: 873-51-8
phenylborondichloride

: 386708-26-5
1,2-dihydro-1-methyl-2-phenyl-1,2-azaborine

Guidance literature:: Multi-step reaction with 6 steps

1: hexane

2: diethyl ether

3: dichloromethane; diethyl ether

4: Bu₄NF / tetrahydrofuran

5: toluene

6: dimethylsulfoxide-d6

With Bu₄NF; In tetrahydrofuran; dimethylsulfoxide-d6; diethyl ether; hexane; dichloromethane; toluene;
DOI:10.1021/om049399g