2,7-Dimethyldecahydronaphthalene

Base Information

• Chemical Name: 2,7-Dimethyldecahydronaphthalene
• CAS No.: 3868-66-4
• Molecular Formula: C12H22
• DSSTox Substance ID: DTXSID30558983
• Mol file: 3868-66-4.mol

Synonyms:decahydro-2,7-dimethylnaphthalene;3868-66-4;2,7-Dimethyldecahydronaphthalene;DTXSID30558983

Chemical Property of 2,7-Dimethyldecahydronaphthalene

Chemical Property:

• XLogP3: 5.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 166.172150702
• Heavy Atom Count: 12
• Complexity: 134

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1CCC2CCC(CC2C1)C

Technology Process of 2,7-Dimethyldecahydronaphthalene

There total 2 articles about 2,7-Dimethyldecahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,7-dimethylnaphthalene (582-16-1) → 2,7-dimethyl-1,2,3,4-tetrahydronaphthalene (13065-07-1,137823-65-5,137823-66-6) + 2,7-dimethyldecaline (3868-66-4)

Guidance literature:

With 1-butyl-1-methylpiperidinium nickel thiotungstate; hydrogen; at 350 ℃; for 10h; under 37503.8 Torr; Autoclave;

DOI:10.1134/S0965544115060110

Reference yield:

cyclohexane (110-82-7,25012-93-5) + acetyl chloride (75-36-5) → 2,7-dimethyldecaline (3868-66-4) + decahydro-2,6-dimethylnaphthalene (1618-22-0) + methyl 2-methylcyclopentyl ketone (1601-00-9)

Guidance literature:

aluminum tri-bromide; In neat (no solvent); at 20 ℃; for 1h; Product distribution; other solvent and temperature;

DOI:10.1016/S0040-4039(01)91337-1

upstream raw materials:

cyclohexane

acetyl chloride

2,7-dimethylnaphthalene