Silane, (ethenyloxy)triethyl-

Base Information

• Chemical Name: Silane, (ethenyloxy)triethyl-
• CAS No.: 3931-86-0
• Molecular Formula: C8H18OSi
• Molecular Weight: 158.316
• DSSTox Substance ID: DTXSID30456773
• Nikkaji Number: J1.455.719I
• Wikidata: Q82279340

Synonyms:Silane, (ethenyloxy)triethyl-;3931-86-0;Vinyloxytriethylsilane;SCHEMBL2116999;DTXSID30456773

Chemical Property of Silane, (ethenyloxy)triethyl-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 5
• Exact Mass: 158.112691728
• Heavy Atom Count: 10
• Complexity: 89.2

Purity/Quality:

99% ,98%,Electron Grade , ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC[Si](CC)(CC)OC=C

Technology Process of Silane, (ethenyloxy)triethyl-

There total 1 articles about Silane, (ethenyloxy)triethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

(C4H9)3SnOCH2CHBrSi(C2H5)3 (59718-66-0) + tributyltin methoxide (1067-52-3) → triethyl-oxiranyl-silane (18388-62-0) + triethylsilyl vinyl ether (3931-86-0) + (Triethylsilyl)-acetaldehyd (59718-69-3) + tributyltin bromide (1461-23-0)

Guidance literature:

170-180°C;

Reference yield: 97.0%

triethylsilyl vinyl ether (3931-86-0) + triethylsilyl trifluoromethyl sulfonate (79271-56-0) + 4-methoxy-benzaldehyde (123-11-5) → 3-(4-methoxyphenyl)-3-((triethylsilyl)oxy)propanal

Guidance literature:

triethylsilyl trifluoromethyl sulfonate; 4-methoxy-benzaldehyde; With [2,2]bipyridinyl; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

triethylsilyl vinyl ether; In dichloromethane; at 0 ℃; for 3h; chemoselective reaction; Inert atmosphere;

DOI:10.1039/c7cc08936h

Reference yield: 72.0%

triethylsilyl vinyl ether (3931-86-0) + acetic acid 4-(tert-butyl-dimethyl-silanyloxy)-6-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-tetrahydro-pyran-2-yl ester (250355-70-5) → {4-(tert-butyl-dimethyl-silanyloxy)-6-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-tetrahydro-pyran-2-yl}-acetaldehyde (250355-71-6)

Guidance literature:

With zinc(II) chloride; In diethyl ether; dichloromethane; for 0.0833333h;

DOI:10.1021/ja011604l

upstream raw materials:

(C₄H₉)3SnOCH₂CHBrSi(C₂H₅)3

tributyltin methoxide

Downstream raw materials:

{4-(tert-butyl-dimethyl-silanyloxy)-6-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-tetrahydro-pyran-2-yl}-acetaldehyde

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