Peroxide, 3-chlorobenzoyl cyclohexylcarbonyl

Base Information

Chemical Name:Peroxide, 3-chlorobenzoyl cyclohexylcarbonyl
CAS No.:39651-57-5
Molecular Formula:C14H15ClO4
Molecular Weight:282.724
Hs Code.:
DSSTox Substance ID:DTXSID80440102
Nikkaji Number:J653.097D
Wikidata:Q82256302

Synonyms:Peroxide, 3-chlorobenzoyl cyclohexylcarbonyl;39651-57-5;SCHEMBL10404925;DTXSID80440102;(3-Chlorobenzoyl)(cyclohexylcarbonyl) peroxide

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Chemical Property of Peroxide, 3-chlorobenzoyl cyclohexylcarbonyl

Chemical Property:

XLogP3:4.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:282.0658866
Heavy Atom Count:19
Complexity:325

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)C(=O)OOC(=O)C2=CC(=CC=C2)Cl

Technology Process of Peroxide, 3-chlorobenzoyl cyclohexylcarbonyl

There total 3 articles about Peroxide, 3-chlorobenzoyl cyclohexylcarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 937-14-4
3-chloro-benzenecarboperoxoic acid

: 2719-27-9
cyclohexanylcarbonyl chloride

: 39651-57-5
3-chlorobenzoic cyclohexanecarboxylic peroxyanhydride

Guidance literature:: With pyridine; In diethyl ether; at -15 ℃; for 1h;
DOI:10.1021/acs.orglett.9b04218

Reference yield:

: 98-89-5
Cyclohexanecarboxylic acid

: 39651-57-5
3-chlorobenzoic cyclohexanecarboxylic peroxyanhydride

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 25 °C

2: pyridine / diethyl ether / 1 h / -15 °C

With pyridine; oxalyl dichloride; N,N-dimethyl-formamide; In diethyl ether; dichloromethane;
DOI:10.1021/acs.orglett.9b04218