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Butanoic acid, 4-[3-[(acetyloxy)(2-phenyl-1,3-dithian-2-yl)methyl]-5-methoxyphenoxy]-, 1,1-dimethylethyl ester

Base Information Edit
  • Chemical Name:Butanoic acid, 4-[3-[(acetyloxy)(2-phenyl-1,3-dithian-2-yl)methyl]-5-methoxyphenoxy]-, 1,1-dimethylethyl ester
  • CAS No.:398142-87-5
  • Molecular Formula:C28H36O6S2
  • Molecular Weight:532.722
  • Hs Code.:
  • Mol file:398142-87-5.mol
Butanoic acid,
4-[3-[(acetyloxy)(2-phenyl-1,3-dithian-2-yl)methyl]-5-methoxyphenoxy]-,
1,1-dimethylethyl ester

Synonyms:

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of Butanoic acid, 4-[3-[(acetyloxy)(2-phenyl-1,3-dithian-2-yl)methyl]-5-methoxyphenoxy]-, 1,1-dimethylethyl ester Edit
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Technology Process of Butanoic acid, 4-[3-[(acetyloxy)(2-phenyl-1,3-dithian-2-yl)methyl]-5-methoxyphenoxy]-, 1,1-dimethylethyl ester

There total 5 articles about Butanoic acid, 4-[3-[(acetyloxy)(2-phenyl-1,3-dithian-2-yl)methyl]-5-methoxyphenoxy]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 3 steps
1.1: n-BuLi / tetrahydrofuran / 1 h / 0 °C
1.2: tetrahydrofuran / 2.5 h / 20 °C
1.3: 80 percent / pyridine / tetrahydrofuran / 0.5 h
2.1: 81 percent / HF*pyr / tetrahydrofuran / 0 °C
3.1: 75 percent / tetrabutylammonium iodide; K2CO3 / acetonitrile / 20 h / 90 °C
With n-butyllithium; tetra-(n-butyl)ammonium iodide; potassium carbonate; pyridine hydrogenfluoride; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo010703e
Guidance literature:
Multi-step reaction with 4 steps
1.1: 93 percent / DIPEA / CH2Cl2; diethyl ether / 24 h
2.1: n-BuLi / tetrahydrofuran / 1 h / 0 °C
2.2: tetrahydrofuran / 2.5 h / 20 °C
2.3: 80 percent / pyridine / tetrahydrofuran / 0.5 h
3.1: 81 percent / HF*pyr / tetrahydrofuran / 0 °C
4.1: 75 percent / tetrabutylammonium iodide; K2CO3 / acetonitrile / 20 h / 90 °C
With n-butyllithium; tetra-(n-butyl)ammonium iodide; potassium carbonate; pyridine hydrogenfluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jo010703e
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