methyl 6-methoxy-5-methylpicolinate

Base Information

Chemical Name:methyl 6-methoxy-5-methylpicolinate
CAS No.:401792-82-3
Molecular Formula:C9H11NO3
Molecular Weight:181.191
Hs Code.:
Mol file:401792-82-3.mol

Synonyms:6-Methoxy-5-methyl-pyridine-2-carboxylic acid methyl ester;Methyl 6-methoxy-5-methylpicolinate;

Suppliers and Price of methyl 6-methoxy-5-methylpicolinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Methyl6-methoxy-5-methylpicolinate 95+%
1g
$ 518.00

Chemenu
methyl6-methoxy-5-methylpicolinate 95%
1g
$ 489.00

Alichem
Methyl6-methoxy-5-methylpicolinate
1g
$ 2808.15

Alichem
Methyl6-methoxy-5-methylpicolinate
500mg
$ 1600.75

Alichem
Methyl6-methoxy-5-methylpicolinate
250mg
$ 1048.60

Total 3 raw suppliers

Chemical Property of methyl 6-methoxy-5-methylpicolinate

Chemical Property:

PSA：48.42000
LogP:1.18520
Storage Temp.:2-8°C

Purity/Quality:

95+% ^*data from raw suppliers

Methyl6-methoxy-5-methylpicolinate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 6-methoxy-5-methylpicolinate

There total 5 articles about methyl 6-methoxy-5-methylpicolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 401792-80-1
methyl 6-hydroxy-5-methyl-2-pyridinecarboxylate

: 74-88-4
methyl iodide

: 401792-82-3
methyl 6-methoxy-5-methyl-2-pyridinecarboxylate

Guidance literature:: With silver carbonate; In chloroform; at 20 ℃; for 120h;
DOI:10.1016/S0957-4166(01)00414-1 DOI:10.1016/S0040-4020(02)00670-1

Reference yield:

: 29681-38-7
methyl 5-methylpyridine-2-carboxylate

: 401792-82-3
methyl 6-methoxy-5-methyl-2-pyridinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 78 percent / m-CPBA / CHCl₃ / 15 h / 20 °C

2.1: Ac₂O / 3 h / Heating

2.2: 51 percent / NaOMe / methanol / 0.17 h / 0 °C

3.1: 93 percent / Ag₂CO₃ / CHCl₃ / 120 h / 20 °C

With acetic anhydride; 3-chloro-benzenecarboperoxoic acid; silver carbonate; In chloroform;
DOI:10.1016/S0040-4020(02)00670-1

Reference yield:

: 589-93-5
2,5-dimethylpyridine

: 401792-82-3
methyl 6-methoxy-5-methyl-2-pyridinecarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: SeO₂ / pyridine / 26 h / Heating

2.1: 8.2 g / conc. H₂SO₄ / 8 h / Heating

3.1: 78 percent / m-CPBA / CHCl₃ / 15 h / 20 °C

4.1: Ac₂O / 3 h / Heating

4.2: 51 percent / NaOMe / methanol / 0.17 h / 0 °C

5.1: 93 percent / Ag₂CO₃ / CHCl₃ / 120 h / 20 °C

With selenium(IV) oxide; sulfuric acid; acetic anhydride; 3-chloro-benzenecarboperoxoic acid; silver carbonate; In pyridine; chloroform;
DOI:10.1016/S0040-4020(02)00670-1